Self-adhesive waterproof roll cementing material and waterproof roll prepared from same
A technology of self-adhesive waterproof membrane and waterproof membrane, which is applied in the direction of adhesives, adhesive types, asphalt material adhesives, etc., can solve the problems of poor flame retardancy of self-adhesive membranes, reduce temperature sensitivity, improve High temperature stability and aging resistance, effect of reducing thermal volatilization
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Embodiment 1
[0029] Organically modified nano palygorskite comprises the following steps:
[0030] A1. Mix 10 mL of HCl solution with a concentration of 0.1 mol / L and 3 g of palygorskite, stir vigorously in a 60°C water bath, and then stand, suction filtration to obtain a solid, wash the solid to neutrality, and vacuum dry at 110°C. to obtain pretreated palygorskite;
[0031] A2. Add 3 g of pretreated palygorskite into 280 mL of xylene, ultrasonically disperse for 0.5 h, add 3 mL of γ-aminopropyltriethoxysilane, heat up to 80 °C, stir at constant temperature for 10 h, and then filter, wash and After vacuum drying at 60°C, the organically modified nano-palygorskite was obtained.
Embodiment 2
[0033] Organically modified nano palygorskite comprises the following steps:
[0034] A1. Mix 15 mL of HCl solution with a concentration of 0.1 mol / L and 3.5 g of palygorskite, stir vigorously in a water bath at 60 °C, and then let stand, suction filtration to obtain a solid, wash the solid to neutrality, and vacuum dry at 110 °C , to obtain pretreated palygorskite;
[0035] A2. Add 4g of pretreated palygorskite into 300mL of xylene, ultrasonically disperse for 0.5h, add 4mL of γ-aminopropyltriethoxysilane, heat up to 80°C, stir at constant temperature for 10h, and then filter, wash and After vacuum drying at 60°C, the organically modified nano-palygorskite was obtained.
Embodiment 3
[0037] Organically modified nano palygorskite comprises the following steps:
[0038] A1. Mix 20 mL of HCl solution with a concentration of 0.1 mol / L and 4 g of palygorskite, stir vigorously in a water bath at 60 °C, then let stand, and filter the solid to obtain a solid. Wash the solid to neutrality, and vacuum dry at 110 °C. to obtain pretreated palygorskite;
[0039] A2. Add 5g of pretreated palygorskite into 320mL of xylene, ultrasonically disperse for 0.5h, add 5mL of γ-aminopropyltriethoxysilane, heat up to 80°C, stir at constant temperature for 10h, and then filter, wash and After vacuum drying at 60°C, the organically modified nano-palygorskite was obtained.
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