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A durable photochromic pet film production process

A technology of photochromism and production technology, which is applied in the field of material science, can solve the problems of unsuitable polyester film production line, unsuitable for large-scale production, and unable to be used in factories, so as to achieve excellent optical performance and avoid uneven and uniform optical performance The effect of strong adhesion

Active Publication Date: 2022-07-29
河南银金达新材料股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Traditional measuring instruments include spectrophotometers, spectrometers, scanning electron microscopes, transmission electron microscopes, diffractometers, etc. These instruments have high measurement accuracy, but are usually expensive, professional, and relatively complicated to operate. They are usually used for product samples. Sampling testing, not suitable for mass production in factory production lines
[0009] In the prior art, there is also a means of rapid detection using image processing methods, but the conventional image processing technology is not specially designed for the difficulties of film detection on the production line, and is not suitable for polyester film production lines. Usually, the detection error rate is high and cannot be detected. actually used in the factory

Method used

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  • A durable photochromic pet film production process
  • A durable photochromic pet film production process
  • A durable photochromic pet film production process

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Experimental program
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Embodiment Construction

[0038] (1) Preparation of photochromic sol solution

[0039] Step 1: WO 3 Preparation of sol: adding Na to ultrapure water 2 WO 4 ·2H 2 O, stir to dissolve, and add mineral acid solution to acidify to PH=4 to obtain WO 3 solution. Adding oxalic acid to ultrapure water to dissolve, heating and stirring during the dissolving process to obtain an oxalic acid solution. The heating temperature is 45-63°C, and the stirring time is 5-10min. will WO 3 Mix the solution with oxalic acid solution, add ultrapure water for dilution and stirring, and form colorless and transparent WO after standing for 6-10h 3 Sol, 0.3M concentration.

[0040] Step 2: TiO 2 Preparation of the sol: The C 16 H 36 O 4 Ti (butyl titanate) was added to anhydrous ethanol, and then ultrapure water was added to the solution to cause a polycondensation reaction to prepare TiO with a sol concentration of 0.3 M 2 sol.

[0041] Step 3: Preparation of ZnO sol: (CH 3 COO) 2 Zn·2H 2 O was dissolved in anh...

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Abstract

A kind of photochromic PET film preparation process that can be durable, including WO 3 , TiO 2 The 8% glycerol solution was added to the composite sol with a molecular ratio of 22:1:1-15:1:1 to ZnO to form a photochromic solution; the PET base film was transferred to the soaking kettle, and after vertical soaking, After oblique soaking, liquid control, and drying, the upper guide roller guides the upper film, and the lower guide roller guides the PET base film and the lower film. The final structure of the three lamination is the upper film-upper photochromic layer-PET Film formation of the base film-under the photochromic layer-under the cover film. The film formed in this way has uniform and excellent optical properties, while avoiding inter-film peeling, and has better durability in use.

Description

technical field [0001] The content of the invention belongs to material science, and in particular, relates to a process for producing a durable photochromic PET film. Background technique [0002] With the continuous development of science and technology and the progress of human society, people's requirements for material materials are also increasing. Among various new materials, photochromic materials are favored by researchers because of their reversible color changes under the irradiation of excitation light. It has huge application prospects in the fields of optical information storage, large-area data display, smart glass and military anti-counterfeiting. [0003] Photochromism is a product that transforms into another color through a series of chemical reactions when a compound is irradiated with light of a certain wavelength; the absorption spectrum changes significantly due to the change of the molecular structure or electronic configuration of the material befor...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B29D7/01
CPCB29D7/01
Inventor 张启纲李沅鸿王威威吴齐蔡文彬袁琳
Owner 河南银金达新材料股份有限公司
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