Fiber master batch with infrared heat storage function and preparation method of fiber master batch
A functional fiber and heat storage technology, applied in the field of textile weaving, can solve the problems of complex preparation process of phase change materials, heavy clothing, and affecting the wearer's activities
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Embodiment 1
[0022] The infrared thermal storage functional fiber masterbatch of the present embodiment is prepared from 2wt% of the concentrated rare earth material and 98 wt% PET, wherein the concentrated rare earth material is calculated by weight including PMA (propylene glycol monomethyl ether acetate) is 100 parts, Cs 0.33 WO 3 For 10 parts, the infrared regenerative rare earth material is 0.5 parts, the dispersant is 6 parts, and the dispersant is polyamide wax; among them, the infrared thermal storage rare earth material is composed of praseodymium hexaborode and lanthanum hexaboride with a weight ratio of 1:1; among them CS 0.33 WO 3 and hexaboride particle size is 140 nm.
[0023] The preparation method of the above infrared thermal storage functional fiber masterbatch includes the following steps:
[0024] (1) Preparation of concentrated rare earth materials:
[0025] Deionized water, cesium tungsten bronze, infrared thermal storage rare earth materials, dispersants are placed in a ...
Embodiment 2
[0032] The infrared thermal storage functional fiber masterbatch of the present embodiment is prepared from 10wt% of the concentrated rare earth material and 90% PE, wherein the concentrated rare earth material is calculated by weight of the number of parts including PMA of 100 parts, Cs 0.33 WO 3 It is 12 parts, the infrared regenerative rare earth material is 0.8 parts, the dispersant is 6 parts, and the dispersant is selected from the polyaminoamide of the cationic unsaturated polycarboxylic acid; among which the infrared thermal storage rare earth material is composed of praseodymium hexaboride, lanthanum hexaboride and cerium hexaboride with a weight ratio of 1:1.5:1; among them CS 0.33 WO 3 The particle size of the hexaborate is 120 nm.
[0033] Infrared thermal storage functional fiber masterbatch and infrared thermal storage functional fiber preparation method with Example 1.
[0034] The density of infrared regenerative rare earth fibers prepared by the testing of the pre...
Embodiment 3
[0036]The infrared thermal storage functional fiber masterbatch of the present embodiment 20wt% of the concentrated rare earth material is prepared with 80% of the PU, wherein the concentrated rare earth material is calculated by weight of the number of parts including 100 parts of PMA, Cs 0.33 WO 3 For 15 parts, infrared regenerative rare earth material is 1 part, dispersant is 6 parts, the dispersant is selected polycarbonyl diimide; among them, the infrared thermal storage rare earth material is composed of praseodymium hexaboride and lanthanum hexaboride with a weight ratio of 1:2; among them, CS 0.33 WO 3 and hexaborate particle size is 100 nm.
[0037] Infrared thermal storage functional fiber masterbatch and infrared thermal storage functional fiber preparation method with Example 1.
[0038] The density of infrared regenerative rare earth fibers prepared by the testing of the present embodiment is 80dtex. After the fibers are woven into the fabric, the fabric structure is ...
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