Polishing pad, manufacturing method of polishing pad, and manufacturing method of semiconductor device
A manufacturing method and technology of polishing pads, which are applied in the field of polishing pads, can solve the problems such as the increase of concaves on the surface of semiconductor wafers, and achieve the effect of preventing defects and increasing the area of direct contact
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Embodiment 1
[0215] Manufacturing of Polishing Pads
[0216] Toluene diisocyanate (TDI), dicyclohexylmethane diisocyanate (H 12 MDI), polytetramethylene ether glycol (Polytetramethylene ether glycol) and diethylene glycol (Diethylene glycol) were put into a four-necked flask, and reacted at 80°C for 3 hours to prepare a preform with an NCO% of 8 to 12%. Polymer (Prepolymer).
[0217] In order to manufacture the polishing layer (Top Pad), in the casting machine (Casting Machine) equipped with prepolymer (Prepolymer), curing agent, inert gas injection pipeline and liquid phase foaming agent injection pipeline, the prepared prepolymer (Prepolymer) is filled in the prepolymer tank (Prepolymer Tank), and the curing agent tank is filled with bis (4-amino-3-chlorophenyl) methane (Bis (4-amino-3-chlorophenyl) methane) (Ishihara (Ishihara) company), while preparing nitrogen (N 2 ) was used as an inert gas, and FC3283 (3M company) was prepared as a liquid-phase blowing agent. Unexpanded solid bl...
Embodiment 2
[0223] It was produced in the same manner as in Example 1, except that unexpanded 031DU40 from AkzoNobel was used as the solid-phase blowing agent. The shell (Shell) component of the solid phase foaming agent is polyvinylidene chloride (Polyvinylidene chloride) or acrylonitrile (Acrylonitrile).
Embodiment 3
[0233] Manufacturing of Polishing Pads
[0234] The TDI, H 12 After MDI, polytetramethylene ether glycol (Polytetramethylene ether glycol) and diethylene glycol (Diethylene glycol) were put into a four-necked flask, they were reacted at 80°C for 3 hours to prepare a prepolymer with an NCO% of 8 to 12%. Material (Prepolymer).
[0235] In order to manufacture the polishing layer (Top Pad), in the casting machine (Casting Machine) equipped with prepolymer, curing agent, inert gas injection pipeline and liquid phase foaming agent injection pipeline, fill the prepared prepolymer into the pre polymer tank, and fill bis(4-amino-3-chlorophenyl)methane (Bis(4-amino-3-chlorophenyl)methane) (Ishihara Company) in the curing agent tank, and prepare nitrogen (N 2 ) was used as an inert gas, and FC3283 (3M company) was prepared as a liquid-phase blowing agent.
[0236] The solid-phase blowing agent (AkzoNobel, 551DU40) and the silicon-based surfactant (Evonik) were mixed into the prepolym...
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