Highly waterproof antibacterial breathable sleeping bag and preparation method thereof
The technology of a sleeping bag and antibacterial liquid is applied in the field of high waterproof, antibacterial and breathable sleeping bag and its preparation, which can solve the problems of endangering the health and reducing the quality of down sleeping bags, and achieve good antibacterial performance, excellent waterproof, antibacterial and breathable performance, and good heat preservation.
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Embodiment 1
[0044] A preparation method of a highly waterproof antibacterial breathable sleeping bag, comprising the following steps:
[0045] Step 1.S11. Add water to the dehydrated down raw material, the bath ratio is 20:1, add biological compound enzyme, degrease at 25°C for 1 hour, filter, and set aside;
[0046] S12. Add the filtered down material to deionized water, add sodium p-aminobenzenesulfonate and cocamidopropyl betaine; soak for 45 minutes, the water temperature is 40°C, filter, and dry at a temperature of 70°C. Get skim down.
[0047] Step 2.S21: prepare antibacterial liquid;
[0048]A. Mix N,N-methylenebisacrylamide and N-methyl-1,3-propanediamine as monomers, feed in a molar ratio of 2:1, dissolve in methanol aqueous solution, protect with nitrogen, and the temperature is 55°C, react for 20 hours, cool naturally, add end-capping agent diethanolamine, the temperature is 40°C, react for 16 hours, concentrate the product by rotary evaporation, add ether to form a precipita...
Embodiment 2
[0058] A preparation method of a highly waterproof antibacterial breathable sleeping bag, comprising the following steps:
[0059] Step 1.S11. Add water to the dehydrated down raw material, the bath ratio is 20:1, add biological compound enzyme, degrease at 27°C for 1.5 hours, filter, and set aside;
[0060] S12. Add the filtered down material to deionized water, add sodium p-aminobenzenesulfonate and cocamidopropyl betaine; soak for 52min, the water temperature is 44°C, filter, and dry at a temperature of 75°C. Get skim down.
[0061] Step 2.S21: prepare antibacterial liquid;
[0062] A. Mix N,N-methylenebisacrylamide and N-methyl-1,3-propanediamine as monomers, feed in a molar ratio of 2:1, dissolve in methanol aqueous solution, protect with nitrogen, and the temperature is 57°C, reacted for 22 hours, cooled naturally, added end-capping agent diethanolamine, the temperature was 42°C, reacted for 17 hours, concentrated the product by rotary evaporation, added ether to form ...
Embodiment 3
[0072] A preparation method of a highly waterproof antibacterial breathable sleeping bag, comprising the following steps:
[0073] Step 1.S11. Add water to the dehydrated down raw material, the bath ratio is 20:1, add biological compound enzyme, degrease at 30°C for 2 hours, filter, and set aside;
[0074] S12. Add the filtered down raw material to deionized water, add sodium p-aminobenzenesulfonate and cocamidopropyl betaine; soak for 60min, the water temperature is 50°C, filter, and dry at 80°C. Get skim down.
[0075] Step 2.S21: prepare antibacterial liquid;
[0076] A. Mix N,N-methylenebisacrylamide and N-methyl-1,3-propanediamine as monomers, feed in a molar ratio of 2:1, dissolve in methanol aqueous solution, protect with nitrogen, and the temperature is 60°C, react for 24 hours, cool naturally, add end-capping agent diethanolamine, the temperature is 45°C, react for 18 hours, concentrate the product by rotary evaporation, add ether to form a precipitate, vacuum dry, ...
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