Flame-retardant coating material for tunnel pavement and preparation method thereof
A coating material and flame-retardant technology, which is applied in the field of flame-retardant coating material for tunnel pavement and its preparation, can solve the problems of application limitation, large smoke generation, etc., achieve good workability, improve stability, The effect of suppressing the spread of combustion
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Embodiment 1
[0078] Embodiment 1: Preparation of modified masterbatch.
[0079] Table 3 Modified masterbatch material ratio and parameter control
[0080]
[0081] Material Description:
[0082] Oleic acid: molecular weight 282.46, melting point 13-14°C;
[0083] Palmitoleic acid: molecular weight 254.41, melting point 0.5°C;
[0084] Soybean oleic acid: 280≤molecular weight≤284, melting point 15℃.
[0085] 【Preparation】
[0086] Add the main solvent 2 and anti-seepage agent in the formula amount into the small reaction kettle, stir at 50°C for 20 minutes to dissolve completely, then add the silane coupling agent and modifier in turn, maintain the temperature and continue stirring for 40 minutes, and naturally drop to After room temperature, ultrasonically treat for a certain period of time to obtain activated modified masterbatches, which are respectively recorded as masterbatch 1, masterbatch 2, masterbatch 3, masterbatch 4, masterbatch 5, masterbatch 6, masterbatch 7, and masterb...
Embodiment 2
[0087] Example 2: Preparation of flame-retardant coating material for tunnel pavement.
[0088] Table 4 Material ratio of coating materials
[0089]
[0090] Material Description:
[0091] Qingchuan Rock Asphalt: Penetration 3 (0.1mm) at 25°C, softening point 220°C;
[0092] 50# asphalt: at 25°C, the penetration is 45 (0.1mm), and the softening point is 67°C;
[0093] 40# asphalt: at 25°C, the penetration is 38 (0.1mm), and the softening point is 70°C;
[0094] 30# asphalt: at 25°C, the penetration is 28 (0.1mm), and the softening point is 72°C;
[0095] 【Preparation】
[0096] A1. Heating the asphalt binder to 135°C, and then cooling to maintain a fluid and transportable state to obtain component A;
[0097] A2. Mix the main solvent 1 with the modified masterbatch at a temperature of 50°C and stir evenly to obtain component B;
[0098] A3. Slowly add component A to the main mixer of component B and mix, then add stabilizer, drier, and functional filler in turn, and st...
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