Ultraviolet light shielding agent composition comprising cerium oxide particles having surface modified with polyhydroxystearic acidand method for preparation of same
A technology of polyhydroxystearic acid and surface modification, which is applied in the field of preparation of ultraviolet shielding agent compositions, can solve the problems of heavy powder texture, unsmooth smearing, stiff use feeling, etc., and achieves low optical refractive index and shielding effect. Outstanding, excellent spreadability
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[0077] The second aspect of the present application provides a method for preparing cerium oxide particles surface-modified by polyhydroxystearic acid, which includes the following steps: mixing polyhydroxystearic acid with a solvent to prepare a mixed solution; The cerium oxide particles are mixed in the mixed solution and milled to prepare cerium oxide particles surface-modified with polyhydroxystearic acid.
[0078] The detailed description of the part that overlaps with the first aspect of the present application is omitted, but even if the description is omitted, the description of the first aspect of the present application can also be applied to the second aspect.
[0079] Below, refer to figure 1 The preparation method of the cerium oxide particles surface-modified with polyhydroxystearic acid in the second aspect of the present application will be described in detail.
[0080] First, in an implementation example of the present application, the preparation method of t...
preparation example
[0096] Preparation Example: Preparation of Cerium Oxide Particles
[0097] To prepare the ultraviolet screener composition of the present invention, cerium oxide particles are prepared.
[0098] After mixing and blending cerium hydroxide, cerium carbonate, cerium nitrate, cerium chloride, and cerium ammonium nitrate, cerium oxide particles are obtained by heat treatment at 400 to 1200°C.
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[0099] Example: Preparation of UV Screening Composition Comprising Cerium Oxide Particles Surface-Modified with Polyhydroxystearic Acid
[0100] Step 1: Preparation of cerium oxide particles surface-modified with polyhydroxystearic acid
[0101] After adding 50 g of polyhydroxystearic acid (polyhydroxystearic acid) to 2,500 g of alkyl benzoate, it stirred. After adding 2,500 g of cerium oxide particles to the solution prepared above, it was milled in a bead mill, followed by dilution to obtain a polyhydroxystearic acid surface-modified cerium oxide dispersion.
[0102] Step 2: Prepare UV Screener Composition
[0103] 200 g of the surface-modified cerium oxide dispersion obtained in the above-mentioned step 1 was dispersed in 800 g of 20% by weight of dibasic alcohol, behenyl alcohol, ethanol and purified water in a ratio of 1:1:2:8 The ratio of the composition of the mixed alcohol solvent to prepare the cerium oxide solution. After that, the above prepared solution (5...
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