A kind of preparation method of composite nanofiber film and flexible strain sensor

A composite nanofiber, strain sensor technology, applied in the direction of fiber processing, fiber type, fiber chemical characteristics, etc., can solve the problems of sensing mechanism failure, weak binding force, reduced sensitivity, etc., to achieve extended strain sensing range, good tension Good elongation and uniformity

Active Publication Date: 2021-12-28
XI AN JIAOTONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, flexible strain sensors prepared in this way usually cannot combine high sensitivity and large detection range
In order to improve the detection range, it is often necessary to increase the amount of conductive nanomaterials, which will lead to a decrease in sensitivity and bring about cost problems
How to prepare flexible sensors with large sensing range and high sensitivity while reducing the amount of expensive conductive nanomaterials is still a big challenge
At the same time, the bonding force between solid conductive nanomaterials and elastic substrates is usually weak, and the conductive network is prone to breakage during the stretching process, which makes the sensing mechanism invalid, resulting in a small sensing range of the flexible strain sensor.
Therefore, while reducing the amount of expensive conductive nanomaterials and ensuring the sensitivity of the sensor, it is still a big challenge to prepare a flexible strain sensor with a large sensing range.

Method used

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  • A kind of preparation method of composite nanofiber film and flexible strain sensor
  • A kind of preparation method of composite nanofiber film and flexible strain sensor
  • A kind of preparation method of composite nanofiber film and flexible strain sensor

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preparation example Construction

[0039] refer to figure 1 , a method for preparing a composite nanofibrous membrane for a flexible strain sensor, comprising the steps of:

[0040] S1. Use a precision balance to measure polymer materials with good tensile strength such as polyurethane particles, polydimethylsiloxane (PDMS) or polyoxymethylene (POM) with a mass fraction of 25% to 30% and add them to the pre-configured In the solvent, use a magnetic stirrer to stir until the polyurethane particles are completely dissolved to obtain a spinning solution;

[0041] S2. Transfer the spinning solution obtained in S1 to the syringe in the electrospinning equipment, extrude the spinning solution through the syringe, adjust the parameters related to electrospinning, so that the extruded spinning solution drops in the high-voltage electrostatic field Under the action, a stable jet is formed, and the jet is stretched at high speed by electric field force, solvent volatilization and solidification, and finally deposited on...

Embodiment 1

[0052] A preparation method for a composite nanofiber membrane for a flexible strain sensor, comprising the following steps:

[0053] A. Use a precision balance to measure polyurethane particles with a mass fraction of 25% and add them to the pre-configured organic solvent. The organic solvent is composed of N,N-dimethylformamide (DMF) solution and acetone solution, wherein N,N- The mass fraction of dimethylformamide (DMF) solution is 75%. Use a magnetic stirrer to stir until the polyurethane particles are completely dissolved to obtain a spinning solution;

[0054] B. Transfer the spinning solution to the syringe, extrude the spinning solution through the syringe, adjust the parameters related to electrospinning, wherein the advancing speed is 6 μL / min, the spinning voltage is 8.65kV, and the receiving distance is 10cm to make the extruded The droplets form a stable jet under the action of a high-voltage electrostatic field, and the jet is stretched at a high speed by the el...

Embodiment 2

[0058] A preparation method for a composite nanofiber membrane for a flexible strain sensor, comprising the following steps:

[0059] A. Use a precision balance to measure polyurethane particles with a mass fraction of 30% and add them to the pre-configured organic solvent. The organic solvent is composed of N,N-dimethylformamide (DMF) solution and acetone solution, wherein N,N- The mass fraction of dimethylformamide (DMF) solution is 60%. Use a magnetic stirrer to stir until the polyurethane particles are completely dissolved to obtain a spinning solution;

[0060] B. Transfer the spinning solution to the syringe, extrude the spinning solution through the syringe, and adjust the parameters related to electrospinning, wherein the advancing speed is 8 μL / min, the spinning voltage is 10 kV, and the receiving distance is 12 cm to make the extruded liquid The droplets form a stable jet under the action of a high-voltage electrostatic field. The jet is stretched at a high speed by...

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Abstract

The invention discloses a preparation method of a composite nanofiber membrane and a flexible strain sensor. The steps of a composite nanofiber membrane are as follows: first dissolving polymer particles in an organic solvent to prepare a spinning solution; transferring the spinning solvent to a syringe In the process, the spinning solution is extruded through a syringe, and the relevant parameters of electrospinning are adjusted to stabilize the jet flow so that the nanofiber film is collected on the collecting plate; after the silver nanowire dispersion is diluted and ultrasonically dispersed in a water bath, vacuum-assisted suction filtration Methods A metal nanowire layer is deposited on the pre-stretched nanofiber film; the bonding force between the nanowires and between the nanowires and the elastic substrate is improved by high temperature annealing. The prepared flexible strain sensor has a large sensing range and can be used to detect deformations such as bending, stretching, and torsion.

Description

technical field [0001] The invention belongs to the technical field of flexible strain sensors, and in particular relates to a preparation method of a composite nanofiber membrane and a flexible strain sensor. Background technique [0002] Strain sensor is a kind of important sensor device. When the sensor device is subjected to external force, it will deform itself, resulting in a change in the resistance or capacitance of the device. By detecting changes in these physical quantities, the function of strain detection is realized. In recent years, flexible and wearable strain sensors have gradually become a research hotspot in the field of strain sensors. This flexible strain sensor has good sensing characteristics such as sensitivity, repeatability and stability, and has become a core device in the fields of electronic skin, wearable electronic devices, and flexible human-computer interaction devices. With the further development of social informatization, various new dev...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06M11/83D01F6/78D01F6/70D04H1/728D01D5/00G01B7/16D06M101/38
CPCD06M11/83D01F6/78D01F6/70D04H1/728D01D5/003G01B7/18
Inventor 方续东孙昊王云凤吴晨康强蒋庄德前田龙太郎
Owner XI AN JIAOTONG UNIV
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