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Liquid plugging agent and preparation method thereof

A plugging agent and liquid technology, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of high risk of water breakthrough, poor oil increase effect, low production, etc., achieve low construction risk, improve adaptability, good The effect of mobility

Inactive Publication Date: 2021-05-04
PETROCHINA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The remaining oil is enriched in the lateral direction of the original fractures, forming a group of low-yield, low-efficiency, and low-production oil wells, which seriously affects the development benefits of the oilfield
Repeated stimulation of old wells has become an important means of treating low-yield and low-efficiency wells. Conventional refracturing technology has long extension of fractures, which makes it easy to communicate with the water injection front, but has a high risk of water breakthrough. It is difficult to realize lateral remaining oil production. Plugging fracturing has gradually become the main means of repeated reconstruction because it can inhibit the extension of fracture length and increase the net pressure inside the seal. However, there are still some problems in temporary plugging fracturing, such as unsatisfactory temporary plugging effect, difficult control of temporary plugging pressure increase, and high construction risk.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A method for preparing a liquid blocking agent,

[0019] The first step, preparation of colloidal particles, dissolve 5-10g of activator in 10-30g of water to obtain an activator solution, add the activator solution to 2-8g of latex, stir until the liquid is clear, and obtain cured colloidal particles ;

[0020] The second step is emulsification of the rubber particles, dissolving 5-10g of the terminator in 20-50g of water, adding the cured rubber particles into the terminator solution, and emulsifying the mixed solution of the rubber particles and the terminator to obtain an emulsion;

[0021] The third step is the preparation of liquid blocking agent. Dissolve 10-15g of stabilizer in 40-60g of water, add the prepared stabilizer solution into the emulsion prepared in the second step, emulsify with emulsifier to obtain the final liquid Blocking agent.

[0022] The activator is ammonium persulfate.

[0023] The terminator is hydroquinone.

[0024] The stabilizer is m...

Embodiment 2

[0029] On the basis of Example 1, step 1: dissolve 5 g of ammonium persulfate in 10 g of water to obtain an ammonium persulfate solution; add the prepared ammonium persulfate solution into 2 g of latex, and use a glass rod to fully Stir until the liquid is clear, and then the cured colloidal particles are obtained.

[0030] Step 2: Dissolve 5 g of hydroquinone in 20 g of water; add the cured colloidal particles into the prepared hydroquinone solution, and use an emulsifier to emulsify the hydroquinone solution added to the colloidal particles After 10 min, the emulsion was obtained.

[0031] Step 3: Dissolve 10 g of montmorillonite in 40 g of water; add the prepared montmorillonite solution into the emulsion prepared in the second step, and use an emulsifier to emulsify for 10 minutes to obtain the final liquid blocking agent. The prepared liquid plugging agent has a viscosity of 28mPa·s, a curing time of 6h, and a working strength of 6Mpa.

Embodiment 3

[0033] On the basis of Example 1, step 1: 10 g of ammonium persulfate is dissolved in 30 g of water to obtain an ammonium persulfate solution; the prepared ammonium persulfate solution is added to 8 g of latex, and the glass rod is used to fully Stir until the liquid is clear, and then the cured colloidal particles are obtained.

[0034] Step 2: Dissolve 10 g of hydroquinone in 50 g of water; add the cured colloidal particles into the prepared hydroquinone solution, and emulsify the hydroquinone solution added to the colloidal particles for 10 min, the emulsion is obtained.

[0035] Step 3: Dissolve 15 g of montmorillonite in 60 g of water; add the prepared montmorillonite solution into the emulsion prepared in the second step, and use an emulsifier to emulsify for 10 minutes to obtain the final liquid blocking agent. The prepared liquid blocking agent has a viscosity of 20mPa·s, a curing time of 7h, and a service strength of 5Mpa.

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Abstract

The invention discloses a liquid plugging agent and a preparation method thereof. The preparation method comprises the following steps: 1, preparing colloidal particles: dissolving 5-10g of an activating agent into 10-30g of water to obtain an activating agent solution, adding the activating agent solution into 2-8g of latex, and stirring until the liquid is clear to obtain cured colloidal particles; 2, emulsifying colloidal particles: dissolving 5-10g of a terminating agent into 20-50g of water, adding the cured colloidal particles into a terminating agent solution, and emulsifying a mixed solution of the colloidal particles and the terminating agent to obtain an emulsion; and 3, preparing the liquid plugging agent: dissolving 10-15g of a stabilizer in 40-60g of water, adding the prepared stabilizer solution into the emulsion prepared in the step 2, and emulsifying by using an emulsifier to obtain a final liquid plugging agent. The prepared emulsion type plugging agent with responsiveness to the pressure difference can form a tough coupling object at the position of the pressure difference, the remaining plugging agent is still kept in a liquid state, good flowability is kept, the adaptive capacity to complex underground conditions is improved, and the construction risk is low.

Description

technical field [0001] The invention belongs to the field of oil field exploration and development. Specifically relates to a liquid blocking agent and a preparation method. Background technique [0002] Some oilfields have the typical characteristics of low pressure, low permeability, and low production. When the oil well was first put into production, it was put into production by conventional sanding fracturing. The sanding fracture was an important seepage channel near the well. Crude oil has been basically produced, but due to low permeability and low formation pressure, it is difficult to recover crude oil from lateral fractures. The remaining oil is enriched in the lateral direction of the original fractures, forming a batch of low-yield, low-efficiency, and low-recovery oil wells, which seriously affects the development benefits of the oilfield. Repeated stimulation of old wells has become an important means of treating low-yield and low-efficiency wells. Conventio...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/508C09K8/88
CPCC09K8/5086C09K8/885
Inventor 张矿生李建辉卜向前吕宝强齐银达引朋卜军王飞吴甫让赵伯平
Owner PETROCHINA CO LTD
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