Material for processing optical element and preparation method thereof

A technology of optical components and raw materials, applied in the direction of adhesive additives, polymer adhesive additives, non-polymer adhesive additives, etc., can solve the problem of increased PV value of optical glass mirror surface shape accuracy, and reduce curing The effect of speed and curing stress, low viscosity and high solvent ratio

Active Publication Date: 2021-04-20
HANGZHOU DIANZI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, during the polishing process, the adhesive is used for bonding and fixing, and the PV value of the optical glass mirror surface shape accuracy increases due to the generation of shrinkage stress.

Method used

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  • Material for processing optical element and preparation method thereof
  • Material for processing optical element and preparation method thereof
  • Material for processing optical element and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0018] The preparation method of above-mentioned optical element processing material, the method concrete steps are as follows:

[0019] Add the above-mentioned components into the stainless steel reaction kettle in sequence according to the amount, heat at 65-75°C, and stir evenly under the protection of nitrogen to obtain the adhesive for polishing and fixing the ground glass.

Embodiment 1

[0027]

[0028] Add the above-mentioned components into a stainless steel reaction kettle in sequence according to the amount, heat at 65° C., and stir evenly under nitrogen protection to obtain the material for optical element processing. Set up 5 groups according to embodiment, its performance is shown in Table 1:

[0029] Table 1.

[0030] serial number Tensile shear strength (MPa) Degumming time (hours) PV value (λ) 1 11.5 4.6 0.07 2 11.0 4.3 0.08 3 10.6 5.2 0.07 4 10.2 6.2 0.04 5 10.6 6.0 0.05

Embodiment 2

[0032]

[0033]

[0034] Add the above-mentioned components into a stainless steel reaction kettle in sequence according to the amount, heat at 65° C., and stir evenly under nitrogen protection to obtain the material for optical element processing. Set up 5 groups according to embodiment, its performance is shown in Table 2:

[0035] Table 2.

[0036] serial number Tensile shear strength (MPa) Degumming time (hours) PV value (λ) 1 10.5 4.6 0.06 2 10.2 5.3 0.07 3 10.5 6.2 0.06 4 11.2 5.2 0.04 5 10.8 6.0 0.04

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Abstract

The invention discloses a material for processing an optical element and a preparation method thereof. The environment-friendly water-based paint is prepared from alpha-cyanoacrylate, acetyl citric acid triester, phosphoric acid tri (2-n-butoxyethyl) ester, trimethylolpropane tri (3-mercaptopropionate), cellulose, fumed silica, tannic acid and phthalic anhydride. The solvent with a branched chain structure and complexing capacity is adopted, the solvent proportion is high, meanwhile, the [alpha]-cyanoacrylate curing speed and curing stress are reduced, and the obtained material for optical element processing has the characteristics of low viscosity, small PV value and proper bonding strength and is suitable for bonding of optical element processing.

Description

technical field [0001] The invention belongs to the technical field of optical precision processing, and in particular relates to a material for optical element processing and a preparation method thereof. Background technique [0002] Optical glass components are widely used in transistors, integrated circuits, printed circuit boards and other semiconductor devices and projectors due to their unique physical and chemical properties, such as high hardness, good optical transparency, various refractive indices, and good homogeneity. Instruments, telescopes, optical microscopes and other optical instruments. Due to the performance requirements of optical components, it is often necessary to strictly polish the frosted glass surface. During the polishing process, the glass to be processed needs to be fixed on a stainless steel mold. In particular, some high-end optical components require high-precision mirror surface shape of optical glass, and its PV value is less than or equ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J4/04C09J11/08C09J11/06C09J11/04
Inventor 聂秋林
Owner HANGZHOU DIANZI UNIV
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