Hot-pressing photon polycrystalline semiconductor material and application thereof
A technology of polycrystalline semiconductors and photons, applied in the field of far-infrared radiation materials, can solve the problems of inability to emit sustainable far-infrared rays, large material mobility, and no mention, so as to promote oxygen-carrying capacity, no ionizing radiation, and maintain The effect of growth
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[0067] A third aspect of the present invention provides a method for preparing a hot-pressed photonic polycrystalline semiconductor material, the preparation method at least including the following steps:
[0068] (1) Mix zirconia, zinc oxide, rare earth salt compounds, and silicate compounds, and fire them in a high-temperature furnace at 1200-1800°C to obtain a fired mixture; transfer the fired mixture to a reaction kettle at a temperature of 800-1200℃, pressure 12.5-25MPa, react in high temperature and high pressure reactor for 40-50h, after cooling, grind to obtain powder material;
[0069] (2) Heat the carrier to 130-180°C, add the surface treatment agent and the powder material prepared in step (1), mix and stir for 15-25 hours, send it into an extruder for extrusion and granulation, and dry it.
Embodiment 1
[0075] The hot-pressed photonic polycrystalline semiconductor material is improved, and the preparation raw materials include 10 parts of zirconia, 5 parts of zinc oxide, 14 parts of rare earth salt compounds, 11 parts of silicate compounds, 1.4 parts of surface treatment agent, and 70 parts of carrier by weight. share.
[0076] The zirconia is nano zirconia.
[0077] The nano-zirconia can be obtained commercially, the manufacturer is Beijing Gaoke New Material Technology Co., Ltd., and the model is GK-ZrO 2 -001.
[0078] The zinc oxide is nano zinc oxide.
[0079] The zinc oxide can be obtained commercially, the manufacturer is Hefei Zhonghang Nano Technology Development Co., Ltd., and the model is ZH-ZnO20N.
[0080] The rare earth salt compound is neodymium chloride, cerium acetate and scandium chloride, wherein the mass ratio of neodymium chloride, cerium acetate and scandium chloride is 1:0.9:1.8.
[0081] The silicate compound is a combination of kaolinite, black to...
Embodiment 2
[0089] The hot-pressed photonic polycrystalline semiconductor material is improved, and the preparation raw materials include 5 parts of zirconia, 2 parts of zinc oxide, 9 parts of rare earth salt compounds, 5 parts of silicate compounds, 0.3 parts of surface treatment agent, and carrier in parts by weight. 60 servings.
[0090] The zirconia is nano zirconia.
[0091] The nano-zirconia can be obtained commercially, the manufacturer is Beijing Gaoke New Material Technology Co., Ltd., and the model is GK-ZrO 2 -001.
[0092] The zinc oxide is nano zinc oxide.
[0093] The zinc oxide can be obtained commercially, the manufacturer is Hefei Zhonghang Nano Technology Development Co., Ltd., and the model is ZH-ZnO20N.
[0094] The rare earth salt compound is neodymium chloride, cerium acetate and scandium chloride, wherein the mass ratio of neodymium chloride, cerium acetate and scandium chloride is 1:0.9:1.8.
[0095] The silicate compound is a combination of kaolinite, black to...
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