Cosmetic preservative removing device
A technology for preservatives and cosmetics, applied in other chemical processes, chemical instruments and methods, liquid separation of solid adsorbents, etc., to achieve the effect of reducing the risk of adverse reactions, reducing the content of preservatives, and improving practicability
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Embodiment 1
[0035] Preparation of Thermally Polymerized Hydroxyethyl Methacrylate / 4-Vinylpyridine (HEMA / VP) Specific Adsorbent (Spherical Particles):
[0036] (1) After mixing 4 g of hydroxyethyl methacrylate and 2 g of 4-vinylpyridine, 0.1 g of cross-linking agent polyethylene glycol dimethacrylate was added while stirring to obtain a mixed solution.
[0037] (2) Pass nitrogen into the mixed solution to remove the dissolved oxygen therein, then add 0.1g initiator azobisisobutyronitrile, and add the solution dropwise to 65°C dimethyl silicone oil under the condition of cutting off oxygen, and heat After 24 hours of polymerization reaction, solidified pellets were obtained.
[0038] (3) Collect the pellets, wash them alternately with distilled water and ethanol, and dry to obtain a HEMA / VP specific adsorbent (spherical particles).
Embodiment 2
[0040] Preparation of Photopolymerized Hydroxyethyl Methacrylate / 4-Vinylpyridine (HEMA / VP) Specific Adsorbent (Spherical Particles):
[0041] (1) After mixing 4 g of hydroxyethyl methacrylate and 2 g of 4-vinylpyridine, 0.1 g of cross-linking agent polyethylene glycol dimethacrylate was added while stirring to obtain a mixed solution.
[0042] (2) Feed nitrogen into the mixed solution to remove dissolved oxygen therein, then add 0.08g initiator 2-p-hydroxyl-2-methyl-1-phenyl-1-acetone, and then dissolve the solution under the condition of cutting off oxygen Add it dropwise into simethicone oil, and irradiate with 365nm ultraviolet rays for 15 minutes at room temperature to obtain cured pellets.
[0043] (3) Collect the pellets, wash them alternately with distilled water and ethanol, and dry to obtain a HEMA / VP specific adsorbent (spherical particles).
Embodiment 3
[0045] The test of the content change of each component after the self-made cosmetic solution flows through the HEMA / VP specific adsorbent:
[0046] In order to illustrate whether the specific adsorbent of the present invention will cause adsorption loss to typical small molecule active ingredients and macromolecular active ingredients in cosmetics while removing paraben ester preservatives. Taking the self-made cosmetic solution as an example, the components of the self-made cosmetic solution are: 1% nicotinamide, 0.2% hyaluronic acid, 0.2% methyl p-hydroxybenzoate, and 0.1% ethyl p-hydroxybenzoate.
[0047] Put 50mL self-made cosmetic solution into a PP bottle; use a PP screen that fits the mouth of the PP bottle to fix the HEMA / VP specific adsorbent provided in Example 1, and then package it in the mouth of the PP bottle. Invert and gently press the PP bottle to pour out the self-made cosmetic solution, simulate the use process, repeat the pouring 5 times, and pour about 10...
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