Thymol composite biological coating preservative and preparation method and application thereof
A technology of coating film preservative and thymol, which is applied in the field of thymol composite bio-coating preservative and its preparation, can solve the problems that the study of edible coating film is still blank, so as to prolong the effective storage period and improve the water solubility. Good effect of property, wettability and solubility
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[0052] The invention also discloses a preparation method of a thymol composite biological coating preservative, comprising the following steps:
[0053] Step 1, prepare thymol microcapsules:
[0054] Step 1.1, Weighing: Weigh the following components according to the following proportions: wall material polyethylene glycol 600027g-111.9g, β-cyclodextrin 111.9g-143.92g, thymol 9.29g-39.17g, sucrose fatty acid glycerin Ester SF15 5g-15g, absolute ethanol is 18.58-78.34ml, the balance is water, the total mass of the above is 1L;
[0055] Step 1.2, take sucrose fatty acid glyceride SF15 and dissolve in distilled water at 85-95°C to obtain a paste solution A with uniform texture;
[0056] Step 1.3, boil water for later use, add polyethylene glycol 6000, homogenize at high speed for 0.5-1.5 minutes, dissolve evenly, degas with ultrasonic to obtain solution B, cool at room temperature for later use;
[0057] Step 1.4. Take β-cyclodextrin and dissolve it in distilled water at 85-95°...
Embodiment 1
[0067] A thymol composite biological coating preservative, containing 0.067g polysaccharide, 0.08g calcium stearoyl lactylate, 0.05g thymol microcapsules in every 1000ml thymol composite biological coating preservative, and the balance is water.
[0068] The polysaccharide includes konjac glucomannan and low-acyl gellan gum with a mass ratio of 1:2; the weight-average average degree of polymerization of the konjac glucomannan is 15 and the weight-average molecular weight is 69030; the low-acyl The weight-average degree of polymerization of gellan gum is 2, and the weight-average molecular weight is 960,000.
[0069] Above-mentioned thymol composite bio-coating preservative is prepared by the following method:
[0070] Step 1, prepare thymol microcapsules:
[0071] Step 1.1. Dissolve 5 g of sucrose fatty acid glyceride SF15 in 250 ml of 90°C distilled water to obtain a paste solution A with uniform texture;
[0072] Step 1.2: Boil 500 ml of water for later use, add 27 ml of p...
Embodiment 2
[0083] A thymol composite biological coating preservative, containing 0.05g polysaccharide, 0.1g calcium stearoyl lactylate, 0.08g thymol microcapsules in every 1000ml thymol composite biological coating preservative, and the balance is water.
[0084] The polysaccharide includes konjac glucomannan and low-acyl gellan gum with a mass ratio of 1:2; the weight-average average degree of polymerization of the konjac glucomannan is 15 and the weight-average molecular weight is 1512836; the low-acyl The weight-average degree of polymerization of gellan gum is 2, and the weight-average molecular weight is 1,107,710.
[0085] Above-mentioned thymol composite bio-coating preservative is prepared by the following method:
[0086] Step 1, prepare thymol microcapsules:
[0087] Step 1.1. Dissolve 10g of sucrose fatty acid glyceride SF15 in 100ml of distilled water at 85°C to obtain a paste solution A with uniform texture;
[0088] Step 1.2, boil water for later use, add 200ml 28.78g pol...
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