High-nickel positive electrode material with rock salt phase thin layer on primary particle surface layer and preparation method thereof
A positive electrode material and surface layer technology, applied in the field of high-nickel positive electrode materials and its preparation, can solve problems such as poor structure and thermal stability
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Embodiment 1
[0042] (1) Weigh NiSO according to the ratio of Ni:Co=9:1 in molar ratio 4 ·6H 2 O and CoSO 4 ·7H 2 O, the total concentration of Ni and Co ions is 4mol L with deionized water -1 mixed salt solution, and then use deionized water to prepare NaOH and ammonia water in a molar ratio of 4:1 to make the NaOH concentration 0.2mol L -1 mixed alkaline solution.
[0043] (2) Add 100 mL of deionized water into the reaction kettle as the reaction base liquid, submerge the deionized water in the stirrer, and add ammonia water to adjust the pH to 11.0. The stirring speed was set to 550 r / min, and the reaction temperature was set to 55°C. Pump the mixed salt solution and mixed alkali solution into the reaction kettle slowly and uniformly, keep the pH stable at 11.0, and the feeding time is 24 hours. After the feeding, continue to pass argon gas and stir for 8 hours. After the reaction is completed, the precipitate is filtered, washed, and dried to obtain a nickel-cobalt positive electr...
Embodiment 2
[0052] (1) Weigh NiSO according to the ratio of Ni:Co=9:1 in molar ratio 4 ·6H 2 O and CoSO 4 ·7H 2 O, the total concentration of Ni and Co ions is 4mol L with deionized water -1 mixed salt solution, and then use deionized water to prepare NaOH and ammonia water in a molar ratio of 4:1 to make the NaOH concentration 0.2mol L -1 mixed alkaline solution.
[0053] (2) Add 100 mL of deionized water into the reaction kettle as the reaction base liquid, submerge the deionized water in the stirrer, and add ammonia water to adjust the pH to 11. The stirring speed was set to 600 r / min, and the reaction temperature was set to 55°C. Pump the mixed salt solution and mixed alkali solution into the reaction kettle slowly and uniformly, keep the pH stable at 11.0, and the feeding time is 24 hours. After the feeding, continue to pass argon gas and stir for 8 hours. After the reaction is completed, the precipitate is filtered, washed, and dried to obtain a nickel-cobalt positive electrod...
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