Preparation method of recyclable and fast demulsification mil-100(fe) composite
A composite material and demulsification technology, which is applied in separation methods, chemical instruments and methods, and immiscible liquid separation, etc., can solve the problems of blank and lack of MIL-100 demulsification research, and achieve ultra-fast demulsification speed and stability Effect of cyclic demulsification ability
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Embodiment 1
[0023] Step 1. Dissolve 0.11g of 1-allyl-3-methylimidazole chloride (AmimCl) in 10ml of water to prepare an aqueous AmimCl solution, and dissolve 0.315g of trimesic acid (BTC) in 10ml of methanol to prepare methanol containing BTC solution;
[0024] Step 2. Get 0.54g ferric chloride hexahydrate (FeCl 3 ·6H 2 O) be dissolved in the 10ml AmimCl aqueous solution prepared by above-mentioned step (1), obtain solution A;
[0025] Step 3. Add 10 ml of the methanol solution containing BTC in step 1 dropwise to the solution A under stirring at room temperature, and the dropping rate is 1-2 drops / second. After the dropwise addition was completed, stirring was continued for 12 hours. The product was centrifuged, washed, dried, and ground to obtain a beige powdery sample, which was the MIL-100(Fe) composite (named Amim@MIL-100(Fe)) anchored by the ionic liquid AmimCl as the positive charge carrier. -1:3).
Embodiment 2
[0027] Step 1. Dissolve 0.228g of 1-allyl-3-methylimidazole chloride (AmimCl) in 10ml of water to prepare an aqueous AmimCl solution, and dissolve 0.315g of trimesic acid (BTC) in 10ml of methanol to prepare methanol containing BTC solution;
[0028] Step 2. Get 0.54g ferric chloride hexahydrate (FeCl 3 ·6H 2 O) be dissolved in the 10ml AmimCl aqueous solution prepared by above-mentioned step (1), obtain solution B;
[0029] Step 3. Add 10 ml of the methanol solution containing BTC in step 1 dropwise to the solution B under stirring at room temperature, and the dropping rate is 1-2 drops / second. After the dropwise addition was completed, stirring was continued for 12 hours. The product was centrifuged, washed, dried, and ground to obtain a beige powdery sample, which was the MIL-100(Fe) composite (named Amim@MIL-100(Fe)) anchored by the ionic liquid AmimCl as the positive charge carrier. -2:3).
Embodiment 3
[0031] Step 1. Dissolve 0.317g of 1-allyl-3-methylimidazole chloride (AmimCl) in 10ml of water to prepare an aqueous AmimCl solution, and dissolve 0.315g of trimesic acid (BTC) in 10ml of methanol to prepare methanol containing BTC solution;
[0032] Step 2. Get 0.54g ferric chloride hexahydrate (FeCl 3 ·6H 2O) be dissolved in the 10ml AmimCl aqueous solution prepared by above-mentioned step (1), obtain solution C;
[0033] Step 3. Add 10 ml of the methanol solution containing BTC in step 1 dropwise to the solution C under stirring at room temperature, and the dropping rate is 1-2 drops / second. After the dropwise addition was completed, stirring was continued for 12 hours. The product was centrifuged, washed, dried, and ground to obtain a beige powdery sample, which was the MIL-100(Fe) composite with ionic liquid AmimCl anchored as a positive charge carrier (named Amim@MIL-100(Fe) ). -3:3).
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