Straight-chain type flame-retardant compound and preparation method thereof
A compound, straight-chain technology, applied in flame-retardant fibers, improved hand fibers, textiles and papermaking, etc., can solve problems such as burning, living and working risks, melting droplets, etc., to reduce contact, reduce possibility, and improve water absorption Effect
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[0049] A kind of preparation method of linear flame retardant compound, it is characterized in that: comprise the following steps:
[0050] Step 1: 20-25 parts by mass of polyvinyl alcohol is heated and dissolved in 180-200 parts by mass of N-methylpyrrolidone solvent to form a saturated solvent; then 30-40 parts by mass of phytic acid, 5- 10 parts by mass of catalyst pyridine, and 30-35 parts by mass of water-absorbing agent dicyclohexylcarbodiimide are added to the solution;
[0051] Step 2: Add the solution formed in Step 1 into the oil bath, and stir until it is completely dissolved;
[0052] Step 3: the solution in step 2 is warmed up to 60 degrees Celsius, this temperature can make the reaction better, continue to stir, react for 4 hours, 4 hours can make the reaction larger;
[0053] Step 4: After cooling the solution in step 3 to room temperature, add 90-100 parts by mass of ethanol precipitation agent to precipitate it, and filter to obtain a white product.
[0054]...
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