Architectural ornament wood-plastic plate for shielding broadband electromagnetic waves and preparation method
An architectural decoration, electromagnetic wave technology, applied in the direction of magnetic/electric field shielding, electrical components, etc., to achieve the effect of broadening the frequency band, enhancing the reflection loss, and overcoming the small dielectric loss
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Embodiment 1
[0034] The preparation process is:
[0035] (1) Dissolve chitosan in acetic acid solution, then add graphene, stir ultrasonically until it is evenly dispersed to obtain a spinning stock solution, then perform wet spinning, and spray it out through a double-ring sleeve-shaped spinneret, Prepare the hollow chitosan fiber of loaded graphene; Wherein, chitosan 32 weight parts, acetic acid solution 120 weight parts, graphene 12 weight parts; The mass concentration of acetic acid solution is 6%; Wet spinning spinneret The pore diameter is 0.4m, the number of holes is 180 holes, and the coagulation bath is a mixed solution of 5wt% NaOH and ETOH;
[0036] (2) Ni (NO 3 ) 2 ·6H 2 O and Fe 2 (NO 3 ) 3 ·6H 2 O is mixed and prepared according to the molar ratio of 1:2, Ni(NO 3 ) 2 ·6H 2 O and Fe 2 (NO 3 ) 3 ·6H 2 O is mixed and formulated into a precursor solution with a mass concentration of 15%. Take 100 parts by weight and then add 37 parts by weight of the graphene-loaded...
Embodiment 2
[0039] The preparation process is:
[0040] (1) Dissolve chitosan in acetic acid solution, then add graphene, stir ultrasonically until it is evenly dispersed to obtain a spinning stock solution, then perform wet spinning, and spray it out through a double-ring sleeve-shaped spinneret, Prepare the hollow chitosan fiber of loading graphene; Wherein, chitosan 30 weight parts, acetic acid solution 130 weight parts, graphene 10 weight parts; The mass concentration of acetic acid solution is 5%; Wet spinning spinneret The pore diameter is 0.3m, the number of holes is 180 holes, and the coagulation bath is a mixed solution of 5wt% NaOH and ETOH;
[0041] (2) Ni (NO 3 ) 2 ·6H 2 O and Fe 2 (NO 3 ) 3 ·6H 2 O is mixed and prepared according to the molar ratio of 1:2, Ni(NO 3 ) 2 ·6H 2 O and Fe 2 (NO 3 ) 3 ·6H 2 O is mixed and formulated into a precursor solution with a mass concentration of 15%. Take 90 parts by weight and then add 40 parts by weight of the graphene-loaded...
Embodiment 3
[0044] The preparation process is:
[0045] (1) Dissolve chitosan in acetic acid solution, then add graphene, stir ultrasonically until it is evenly dispersed to obtain a spinning stock solution, then perform wet spinning, and spray it out through a double-ring sleeve-shaped spinneret, Prepare the hollow chitosan fiber of loading graphene; Wherein, chitosan 34 weight parts, acetic acid solution 120 weight parts, graphene 13 weight parts; The mass concentration of acetic acid solution is 7%; Wet spinning spinneret The pore diameter is 0.5m, the number of holes is 180 holes, and the coagulation bath is a mixed solution of 6wt% NaOH and ETOH;
[0046] (2) Ni (NO 3 ) 2 ·6H 2 O and Fe 2 (NO 3 ) 3 ·6H 2 O is mixed and prepared according to the molar ratio of 1:2, Ni(NO 3 ) 2 ·6H 2 O and Fe 2 (NO 3 ) 3 ·6H 2 O mixed and prepared into a precursor solution with a mass concentration of 15%, take 100 parts by weight, and then add 33 parts by weight of the graphene-loaded ho...
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