Preparation method of light-transmitting heat-insulating glass
A technology of insulating glass and preparation steps, applied in the direction of coating, etc., can solve the problems of general thermal insulation performance and light transmission of insulating glass, and achieve the effects of reducing the induced dipole moment, narrowing the particle size distribution, and reducing scattering
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Embodiment 1
[0034] The silane coupling agent is: γ-aminopropyltriethoxysilane
[0035] Preparation of the dispersion:
[0036] In terms of parts by weight, add 30 parts of absolute ethanol and 5 powders of hydroxyapatite powder to the ultrasonic oscillator, and use the frequency of 30kHz to ultrasonically vibrate for 5min to obtain a suspension, which is placed in a cone with a stirrer In the conical flask, add 18 parts of tetrabutyl titanate to the Erlenmeyer flask at a dropping rate of 4 mL / min with a dropping funnel, start the stirrer at the same time, and start stirring at a speed of 300 r / min for 10 min to obtain a dispersion;
[0037] Preparation of silicon-titanium composite rubber powder:
[0038] In parts by weight, add 4 parts of acetic acid solution with a mass fraction of 20% and 20 parts of silica sol to 80 parts of the above-mentioned dispersion liquid, stir and disperse for 1 hour, and then stand and age for 2 days to obtain a dry sol. The dry sol was air-dried in a hot a...
Embodiment 2
[0049] The silane coupling agent is: γ-(2,3-epoxypropoxy)propyltrimethoxysilane
[0050] Preparation of the dispersion:
[0051] In parts by weight, add 35 parts of absolute ethanol and 6 powders of hydroxyapatite powder to the ultrasonic oscillator, with a frequency of 32.5kHz, ultrasonic vibration for 6min to obtain a suspension, which is placed in a mixer with a stirrer In the Erlenmeyer flask, add 19 parts of tetrabutyl titanate into the Erlenmeyer flask at a dropping rate of 4.5mL / min with a dropping funnel, start the stirrer at the same time, start stirring at a speed of 350r / min for 12.5min to obtain a dispersion ;
[0052] Preparation of silicon-titanium composite rubber powder:
[0053] In terms of parts by weight, add 4.5 parts of acetic acid solution and 25 parts of silica sol with a mass fraction of 20% to 85 parts of the above-mentioned dispersion liquid, stir and disperse for 1.5 hours, and then stand and age for 2.5 days to obtain a dry sol. The obtained dry ...
Embodiment 3
[0064] The silane coupling agent is: γ-methacryloxypropyltrimethoxysilane
[0065] Preparation of the dispersion:
[0066] In parts by weight, add 40 parts of absolute ethanol and 7 powders of hydroxyapatite powder to the ultrasonic oscillator, and ultrasonically vibrate for 7 minutes at a frequency of 35 kHz to obtain a suspension, which is placed in a cone with a stirrer In the conical flask, add 20 parts of tetrabutyl titanate to the Erlenmeyer flask with a dropping funnel at a dropping rate of 5mL / min, start the stirrer at the same time, start stirring at a speed of 400r / min for 15min to obtain a dispersion;
[0067] Preparation of silicon-titanium composite rubber powder:
[0068] In parts by weight, 5 parts of acetic acid solution with a mass fraction of 20% and 30 parts of silica sol were added to 90 parts of the above-mentioned dispersion liquid, stirred and dispersed for 2 hours, and left to stand for aging for 3 days to obtain a dry sol. The dry sol was air-dried i...
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