A kind of insect trapping microcapsule which can be used for sticky insect board and its preparation method and application
A technology of microcapsules and insect sticky boards, applied in botany equipment and methods, chemicals for biological control, applications, etc., can solve the problems of reduced adhesion of adhesives, achieve stable emission speed, and long-term insect trapping , Good lure distribution effect
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Embodiment 1
[0032] (1) prepare double emulsion:
[0033] A tapered cylindrical glass capillary with an inner diameter of 60 μm, an outer diameter of 150 μm, and an inner diameter of 4 μm at the tip is nested in a square glass tube with an inner side length of 180 μm and an outer side length of 300 μm and is coaxial with the square glass tube. Then align the inlet of the collection tube with an inner diameter of 60 μm, an outer diameter of 150 μm, and an inlet inner diameter of 20 μm with the tip of the tapered cylindrical glass capillary, nested in the square glass tube and coaxial with the square glass tube. The preparation equipment used to form the double emulsion.
[0034]An aqueous solution containing 1.5wt% methylcellulose as the outermost fluid; fluorinated acrylate, methyl methacrylate, acrylic acid, N,N-methylenebisacrylamide, benzoyl peroxide and phthalic acid Diethyl ester is mixed at a mass ratio of 1:10:12:0.5:0.05:5 as the middle phase fluid; water is the innermost phase fl...
Embodiment 2
[0042] (1) prepare double emulsion:
[0043] A tapered cylindrical glass capillary with an inner diameter of 60 μm, an outer diameter of 150 μm, and an inner diameter of 4 μm at the tip is nested in a square glass tube with an inner side length of 180 μm and an outer side length of 300 μm and is coaxial with the square glass tube. Then align the inlet of the collection tube with an inner diameter of 60 μm, an outer diameter of 150 μm, and an inlet inner diameter of 20 μm with the tip of the tapered cylindrical glass capillary, nested in the square glass tube and coaxial with the square glass tube. The preparation equipment used to form the double emulsion.
[0044] An aqueous solution containing 2.5wt% polyvinyl alcohol is the outermost fluid; fluorine-containing acrylate, methyl methacrylate, acrylic acid, N,N-methylenebisacrylamide, benzoyl peroxide and pentane according to 1: The mass ratio of 15:14:0.8:0.08:9 is mixed as the mesophase fluid; water is the innermost phase f...
Embodiment 3
[0052] (1) prepare double emulsion:
[0053] A tapered cylindrical glass capillary with an inner diameter of 200 μm, an outer diameter of 350 μm, and an inner diameter of 30 μm at the tip is nested in a square glass tube with an inner side length of 400 μm and an outer side length of 550 μm and is coaxial with the square glass tube. Then align the inlet of the collection tube with an inner diameter of 200 μm, an outer diameter of 350 μm, and an inlet inner diameter of 50 μm with the tip of the tapered cylindrical glass capillary, nested in the square glass tube and coaxial with the square glass tube. The preparation equipment used to form the double emulsion.
[0054] The aqueous solution containing 2wt% sodium polyacrylate is the outermost fluid; : 10: 12: 0.9: 0.06: 8 The mass ratio is mixed as the mesophase fluid; water is the innermost phase fluid. Use a microsyringe pump to deliver the innermost phase fluid into the tapered cylindrical capillary at a rate of 2mL / hr, and...
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