Preparation method of cigarette butt tar extract with aroma characteristic and application of cigarette butt tar extract in cigarettes

A technology of extracts and cigarettes, applied in the field of tobacco technology, to achieve the effects of low cost, solving the lack of smoke, and avoiding environmental pollution

Active Publication Date: 2020-04-21
INNER MONGOLIA KUNMING CIGARETTE CO LTD
View PDF6 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This patent uses the waste tobacco powder produced in the cigarette production process as raw material, and the waste tobacco powder does not contain tar components, and does not involve the preparation method of tar extract

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Preparation method of cigarette butt tar extract with aroma characteristic and application of cigarette butt tar extract in cigarettes
  • Preparation method of cigarette butt tar extract with aroma characteristic and application of cigarette butt tar extract in cigarettes
  • Preparation method of cigarette butt tar extract with aroma characteristic and application of cigarette butt tar extract in cigarettes

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Example 1 Preparation of cigarette tar extract

[0029] A method for preparing a cigarette butt tar extract with aroma-inducing properties comprises the following steps:

[0030] (1) Pretreatment of cigarette butts: tear off the outer wrapping paper of cigarette butts, and cut the tow into small sections less than 1 cm in length;

[0031] (2) Add 100 g of the pretreated cigarette butts into 1 L of absolute ethanol, extract in a reflux water bath at 60° C. for 4 h, and centrifuge at 1000 r / min for 2 min to obtain an extract;

[0032] (3) Distill the extract under reduced pressure with a water pump to remove the organic solvent, then connect it to an oil pump vacuum system, adjust the pressure to 0.5mmH, heat slowly, and collect fractions below 200°C;

[0033] (4) The collected fractions were extracted 3 times with chloroform, the extracts were combined, then concentrated and desolvated on a rotary evaporator, the temperature was controlled at 45 ° C, the pressure was 2...

Embodiment 2

[0052] Example 2 Aroma-inducing properties of cigarette tar extract

[0053] The heat-not-burn cigarette sample A (HnB sample A) was prepared by adding the tar extract prepared in Example 1 to the condensation auxiliary material of the heat-not-burn cigarette at an addition ratio of 3% by weight of the heat-not-burn cigarette.

[0054] The tar extract prepared in Example 1 was added to the filter auxiliary material of the heat-not-burn cigarette at an addition rate of 2% by weight of the heat-not-burn cigarette to prepare the heat-not-burn cigarette sample B (HnB sample B).

[0055]Heat-not-burn cigarette sample C (HnB sample C) was prepared by adding the tar extract prepared in Example 1 to reconstituted shredded tobacco of heat-not-burn cigarettes at an addition ratio of 4% by weight of heat-not-burn cigarettes.

[0056] After the cigarette samples made by the above scheme and the cigarettes without tar extract were balanced for 24 hours in a constant temperature and humid...

Embodiment 3

[0060] Example 3 Selection of preparation method conditions

[0061] 1. Selection of organic solvents

[0062] Use methanol, dichloromethane, absolute ethanol, glycerin, petroleum ether, polyethylene glycol 400 to extract the pretreated cigarette butts, the ratio of solid to liquid is 1:10 (g / mL), the extraction time is 2 hours, and the water bath The temperature was 60°C, and the extraction was performed once. The influence of different solvents on the extraction effect (the content of the extracted components per g of cigarette butt) was compared and analyzed. The test results are shown in Table 2. It can be seen from Table 2 that the extraction effect is the best when using absolute ethanol.

[0063] Extraction effect (mg / g) of different organic solvents of table 2

[0064]

[0065] 2. Selection of extraction temperature

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention provides a method for preparing a cigarette butt tar extract with an aroma characteristic and application of the cigarette butt tar extract in cigarettes, and the method comprises the following steps: (1) adding cigarette butts into an organic solvent for extraction, and centrifuging after extraction to obtain an extracting solution; and (2) distilling the extracting solution under reduced pressure to remove the organic solvent, distilling under vacuum pressure, and collecting fractions below 200 DEG C to obtain the tar extract. Waste cigarette butts are used as raw materials, and organic solvent extraction and reduced pressure distillation separation are used, so that harmful substances in waste cigarette butt tar are removed, and aroma characteristic components of the wastecigarette butt tar are reserved; by applying the cigarette butt tar extract to heat-not-burn cigarettes, aroma, smoke and taste characteristics of the heat-not-burn cigarettes are improved, and the problem that the heat-not-burn cigarette is dull in cigarette smell or poor in aroma puff-by-puff release stability is effectively solved.

Description

technical field [0001] The invention relates to a method for preparing a tar extract with aroma-inducing properties from waste cigarette butts and its application in cigarettes, belonging to the technical field of tobacco technology. Background technique [0002] Cigarettes refer to tobacco products in which shredded tobacco is rolled into strips with cigarette paper. Cigarettes are mainly composed of four parts: shredded tobacco, cigarette paper, tipping paper and filter. Cigarette paper (also known as coil paper) is a special paper for wrapping shredded tobacco; tipping paper (also known as tipping paper) is a special paper for connecting cigarettes and filters. The tipping paper and the filter part make up the cigarette butt. Cigarette butt refers to the remaining part of cigarette after burning. The cigarette butt is composed of the outer wrapping paper and the bundle inside the fiber filament. The fiber bundle of the cigarette butt has adsorption capacity and can eff...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): A24B15/24A24B3/12
CPCA24B15/24A24B3/12
Inventor 李力群郭春生郝捷张峻松纪旭东叶亚军陈晨田数王旭东乔月梅李瑞丽梁淼张文洁
Owner INNER MONGOLIA KUNMING CIGARETTE CO LTD
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap