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Template for duplicating hydrophobic coating

A hydrophobic coating and template technology, applied in the field of materials, can solve the problems of not being suitable for large-scale production, difficult to control the etching effect, complicated preparation process, etc., and achieve good industrial application prospects, low cost, and enhanced hydrophobicity of the coating Effect

Active Publication Date: 2020-02-07
EAST CHINA UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The size of the surface roughness of the material can be well controlled by photolithography, but the instrument is expensive and the preparation process is complicated, so it is not suitable for large-scale production; the publication number is CN103409754A, and the name is "Surface Ultrasonic Technology of Aluminum Materials Based on Etching Method". The invention of Hydrophobic Treatment Process” reported that a certain concentration of hydrochloric acid solution was used to etch the surface of polished aluminum samples, and then modified with stearic acid ethanol solution to obtain superhydrophobic properties.
Etching porous aluminum templates can construct roughness, but the choice of substrates is limited, and the etching effect is not easy to control

Method used

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  • Template for duplicating hydrophobic coating
  • Template for duplicating hydrophobic coating
  • Template for duplicating hydrophobic coating

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Dissolve 30g of vinyl silicone resin in 70.5g of xylene, stir well, add 0.06g of defoamer (BYK-306), 0.06g of leveling agent (BYK-333), 0.2g of dibutyltin dilaurate After stirring evenly again, put it into a 90°C oven and keep it warm for 4 hours to pre-cure it to obtain a template material.

[0031] Get 20g of ammonium chloride and 15g of sodium chloride and dissolve in 200g of deionized water. Adjust the pressure of the air compressor to 0.2MPa, atomize the solution through a spray gun, spray on the surface of the template material twice, and after the salt particles crystallize, heat the template material to 170°C for 2 hours. After the curing is complete, the template material is placed in deionized water to etch away the salt particles, and finally a template for hydrophobic coating replication is obtained.

[0032] Pour an E51 epoxy resin coating with a thickness of about 1 mm on the surface of the formwork, and release it after curing to obtain an epoxy resin co...

Embodiment 2

[0035] Dissolve 10g of phenyl silicone resin and 15g of vinyl silicone resin in 74.4g of xylene, stir well, add 0.2g of defoamer (BYK-A535), 0.2g of leveling agent (BYK-380N), 0.2g of sulfur Dioctyltin alcohol, stirred evenly again, put it into an oven at 80°C for 8 hours to keep it warm for pre-curing to obtain a template material.

[0036] Dissolve 35g of potassium carbonate in 100g of deionized water. Adjust the pressure of the air compressor to 0.8MPa, atomize the solution through a spray gun, and spray it on the surface of the resin for 4 times, after potassium carbonate crystallizes. Heat the template material to 220°C for 2h. After curing is complete, the template material is placed in deionized water to etch away the salt particles, and finally a template for hydrophobic coating replication is obtained.

[0037] Pouring a polydimethylsiloxane coating with a thickness of about 1 mm on the surface of the formwork, and demoulding after curing, a polydimethylsiloxane coa...

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PUM

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Abstract

The invention discloses a template for duplicating a hydrophobic coating. The template is prepared with a method comprising the step as follows: firstly, a template material is prepared, and raw materials of the template comprise 40-70 parts of silicone resin, 0.01-10 parts of a leveling agent, 0.01-10 parts of a defoaming agent, 0.01-5 parts of a catalyst and 20-50 parts of a solvent. After the silicone resin is dissolved in a solvent in proportion, the defoaming agent, the leveling agent and the catalyst are added and stirred uniformly, heat preservation is performed at the temperature of 40-100 DEG C for 1-8 h, and the template material for duplicating the hydrophobic coating is obtained; and then the surface of the template material is etched: soluble salt is inlaid in the surface layer of the template material in a repeated spraying mode, salt particles are etched, a multi-stage coarse structure is formed on the surface of a matrix simply and rapidly, and the template for duplicating the hydrophobic coating is prepared. The template adopts a simple process, has low production cost, is green and environmentally friendly, and can be recycled.

Description

technical field [0001] The invention relates to a template for hydrophobic coating replication. It belongs to the field of material technology. Background technique [0002] Hydrophobic materials have important applications in many occasions, for example, they can be used for anti-fouling self-cleaning, anti-icing, anti-corrosion, anti-oxidation, and prevention of current conduction, etc. Based on the hydrophobic self-cleaning effect of lotus leaves, bionic-based superhydrophobic surfaces have become a research hotspot. When preparing a hydrophobic surface, the free energy of the material surface must first be reduced; secondly, increasing the surface roughness of the material and reducing the contact area between water droplets and the surface can effectively increase the surface contact angle and increase hydrophobicity. [0003] However, the current surface roughness construction methods still have many problems such as complex process and high cost. For example: the i...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L83/07C08L83/04C08J7/00
CPCC08J7/00C08J2383/04C08J2383/07
Inventor 张衍朱鑫睿刘育建
Owner EAST CHINA UNIV OF SCI & TECH
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