Tin sulfide-nickel sulfide heterogeneous nanosheet array structure and preparation method thereof
A nanosheet array, tin sulfide technology, applied in nickel sulfide, chemical instruments and methods, nanotechnology, etc., to achieve the effects of excellent electrochemical energy storage performance, controllable morphology, and large output
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[0030] The preparation method of the uniform composite tin sulfide-nickel sulfide heterogeneous nanosheet array structure supported on the surface of the conductive substrate proposed by the present invention comprises the following steps and contents:
[0031] (1) In a beaker, first add tin tetrachloride, nickel chloride and thioacetamide, then add alcohol solvent, stir well to make it evenly mixed. Then add deionized water and continue to stir until it becomes a clear light green solution.
[0032] (2) Transfer the above solution to the reaction kettle, insert the pre-washed conductive substrate vertically, seal it and put it into the electric furnace, then heat it from room temperature to 140-180°C at a rate of 5-20°C / min, and keep it warm 4-12 hours. After naturally cooling to room temperature, open the reactor, take out the substrate, alternately rinse with deionized water and alcohol for 3-5 times, and dry at 50-80°C for 8-12 hours to obtain the , Uniform composite tin...
Embodiment 1
[0039] Example 1: In a 100mL beaker, add 0.631g of tin tetrachloride pentahydrate, 0.285g of nickel chloride hexahydrate and 0.451g of thioacetamide; then add 59mL of alcohol, stir well to make it evenly mixed; then add 1mL to Ionized water, continue to stir for 20 minutes until it becomes a clear light green solution.
[0040] Then the above solution was transferred to the reaction kettle, and a pre-washed carbon cloth (3.7×5cm 2 ) piece, sealed and placed in an electric furnace, then heated from room temperature to 160°C at a rate of 15°C / min, and kept for 8 hours. After naturally cooling to room temperature, open the reaction kettle, take out the carbon cloth, rinse it with deionized water and alcohol alternately for 5 times, and dry it at 60°C for 12 hours to obtain the carbon cloth-supported tin sulfide-nickel sulfide heterogeneous nanosheets array structure.
[0041] X-ray diffraction analysis shows that the black product is SnS loaded on the surface of carbon cloth 2...
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