Efficient water purifying agent and preparation method thereof
A water purifying agent, high-efficiency technology, applied in the direction of chemical instruments and methods, water pollutants, water/sewage treatment, etc., can solve the problems of complex equipment, large dosage, and various types, and achieve improved adsorption performance and unique Secondary pollution and low treatment cost
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Embodiment 1
[0023] Embodiment 1: Preparation of attapulgite composite active particles
[0024] Mix attapulgite with hydrochloric acid solution with a concentration of 5mol / L at a ratio of 1g / 10mL, stir and heat to 100°C, activate for 5h, after the reaction, wash with water until the pH is 5.5, centrifuge, and remove the precipitate at 110 Dry at ℃ for 12 hours to obtain pretreated attapulgite, mix the pretreated attapulgite with 20% choline solution in a mass ratio of 3:1, granulate, and activate at 120°C for 2 hours to obtain Attapulgite composite active particles.
Embodiment 2
[0025] Embodiment 2: Preparation of attapulgite composite active particles
[0026] Mix attapulgite with hydrochloric acid solution with a concentration of 5mol / L at a ratio of 1g / 10mL, stir and heat to 100°C, activate for 5h, after the reaction, wash with water until the pH is 5.5, centrifuge, and remove the precipitate at 110 Dry at ℃ for 12 hours to obtain pretreated attapulgite, mix the pretreated attapulgite with 10% choline solution in a mass ratio of 2:1, granulate, and activate at 180°C for 1 hour to obtain Attapulgite composite active particles.
Embodiment 3
[0027] Embodiment 3: Preparation of hyperbranched polyethyleneimine grafted psyllium husk fiber
[0028] (1) Preparation of pretreated psyllium seed husk fiber: the psyllium seed husk powder is added to the sodium hydroxide solution with a mass fraction of 2%, and the mass ratio of the psyllium seed husk powder and the sodium hydroxide solution is 1 : 15; heat treatment 3h at 100 DEG C, cooling, solid-liquid separation, washing deposit, drying, obtains the psyllium seed husk cellulose, and the psyllium seed husk cellulose is added the hydrogen peroxide solution that molar concentration is 0.5mol / L Among them, the mass ratio of the psyllium seed husk cellulose to the hydrogen peroxide solution is 1:2, react at 60°C for 3h under stirring conditions, separate the solid from the liquid, wash the precipitate, dry it, grind it for later use, and obtain the pretreated Psyllium Husk Fiber.
[0029] (2) Preparation of hyperbranched polyethyleneimine grafted psyllium seed husk fiber: t...
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