Magnetic sieve plate and preparation method and use method thereof
A sieve plate and magnetic technology, applied in the field of magnetic sieve plate and its preparation, can solve the problems of inability to disassemble, large pore size of magnetic sieve plate, difficult to clean, etc., and achieve the effect of simple preparation method, uniform magnetic distribution and good filtering effect
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Embodiment 1
[0065] A kind of magnetic sieve plate, its preparation method specifically comprises the following steps:
[0066] (1) Dissolve 5.42g of ferric chloride hexahydrate and 2.356g of ferrous chloride tetrahydrate in 10ml of ultrapure water, mix them, and vortex evenly; pour them into a mixture of 100ml of ultrapure water and 15ml of ammonia water, 300rpm Stir mechanically, wash to neutral after reacting for 30 minutes, and obtain ferroferric oxide magnetic beads;
[0067] (2) Mix 0.3g of ferroferric oxide magnetic beads with 4g of styrene, 6g of polyvinylpyrrolidone, and 80ml of water, evacuate nitrogen and remove oxygen; stir at 600rpm and heat up to 82°C, pour 0.2g of benzyl oxide after the temperature stabilizes acyl, reacted for 48 hours; magnetic polystyrene microspheres were collected by washing with a magnet;
[0068] (3) The magnetic microspheres were stacked in the center of a 5000-mesh porous metal-based filter plate, and pressed at 110° C. with a pressure of 4 tons to ...
Embodiment 2
[0071] A kind of magnetic sieve plate, its preparation method specifically comprises the following steps:
[0072] (1) Put polyethylene powder into the mold, place the mold in a hot press, press the upper and lower plates at a temperature of 230°C, press at 3MPa for 60 minutes, and then air cool to room temperature to obtain a filter plate;
[0073] (2) Dissolve 5.42g of ferric chloride hexahydrate and 2.356g of ferrous chloride tetrahydrate in 10ml of ultrapure water and mix them, vortex evenly; pour into the mixture of 100ml of ultrapure water and 15ml of ammonia water, 300rpm Stir mechanically, wash to neutral after reacting for 30 minutes, and obtain ferric oxide magnetic beads; disperse the ferric ferric oxide magnetic beads in aqueous ethanol to form a magnetic bead dispersion;
[0074] (3) Mix 10 g of the filter plate with 1 g of the magnetic bead dispersion, reflux for 60 minutes, and dry to obtain the magnetic sieve plate.
[0075] The method of using the magnetic si...
Embodiment 3
[0077] A kind of magnetic sieve plate, its preparation method specifically comprises the following steps:
[0078] (1) Dissolve 5.42g of ferric chloride hexahydrate and 2.356g of ferrous chloride tetrahydrate in 10ml of ultrapure water, mix them, and vortex evenly; pour them into a mixture of 100ml of ultrapure water and 15ml of ammonia water, 300rpm Stir mechanically, wash to neutral after reacting for 30 minutes, and obtain ferroferric oxide magnetic beads;
[0079] (2) Mix 0.3g of ferroferric oxide magnetic beads with 4g of styrene, 6g of polyvinylpyrrolidone, and 80ml of water, evacuate nitrogen and remove oxygen; stir at 600rpm and heat up to 82°C, pour 0.2g of benzyl oxide after the temperature stabilizes acyl, reacted for 48 hours; magnetic polystyrene microspheres were collected by washing with a magnet;
[0080](3) Put the magnetic polystyrene microspheres in a metal mold, put the metal mold in a hot press, press the upper and lower plates at a temperature of 170°C, ...
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