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Sound-insulation heat-preservation rubber product and preparation method thereof

A technology for rubber products, sound insulation and heat preservation, applied in the rubber field, can solve the problems of poor mechanical properties, vulcanization performance and aging resistance, poor dispersion of filler calcium carbonate, poor mechanical properties of silica aerogel, etc., to improve mechanical properties, The effect of improving dispersibility

Active Publication Date: 2019-10-25
南京大毛牛环保科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Moreover, because silica airgel has the properties of sound insulation and heat preservation, ethylene-propylene rubber is mostly used in conjunction with silica airgel to prepare rubber products with sound insulation and heat preservation; but in the process of preparing rubber products, silica gas condensation The poor mechanical properties of the rubber and the poor dispersibility of the filler calcium carbonate in the reaction system lead to the disadvantages of poor mechanical properties, vulcanization properties, and aging resistance of rubber products, thus becoming the focus of the present invention's research

Method used

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  • Sound-insulation heat-preservation rubber product and preparation method thereof

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preparation example Construction

[0078] A second aspect of the present invention provides a method for preparing a sound-insulating and heat-insulating rubber product, comprising the following steps:

[0079] (1) Put the EPDM rubber of the above-mentioned parts by weight into an open mill and carry out plasticizing and wrapping rolls to obtain rubber compound 1;

[0080] (2) Add the silica airgel, filler, sulfur, vulcanization accelerator, activator, plasticizer, anti-aging agent, organic foaming agent, paraffin oil of the above-mentioned parts by weight to the rubber material 1 obtained in step (1) In the middle, then the film is removed and parked for 45-55h to obtain the rubber compound 2, and finally the rubber compound 2 is re-milled to obtain the rubber compound 3;

Embodiment 1

[0085] Embodiment 1 provides a sound-insulating and heat-insulating rubber product. In parts by weight, the preparation raw materials include at least: 80 parts of EPDM rubber, 20 parts of silica airgel, 15 parts of filler, 0.5 part of sulfur, and activator 1 part, 1 part of plasticizer, 1 part of anti-aging agent, 2 parts of organic foaming agent, 20 parts of paraffin oil.

[0086] The EPDM rubber is ethylidene norbornene type EPDM rubber.

[0087] The silica airgel is (methoxycarbonylaminomethyl)trimethoxysilane modified silica airgel.

[0088] In one embodiment, the preparation method of the (methoxycarbonylaminomethyl)trimethoxysilane modified silica airgel is: at room temperature, 10mL (methoxycarbonylaminomethyl)trimethoxy Mix silane coupling agent, 90mL n-hexane, and 5mL hydrochloric acid evenly to prepare a surface modification solution, then immerse 200mg of silica airgel in the surface modification solution, let it stand for reaction, filter to obtain a precipitate,...

Embodiment 2

[0100] Embodiment 2 provides a sound-insulating and heat-insulating rubber product. In parts by weight, the preparation raw materials include at least: 90 parts of EPDM rubber, 22 parts of silica airgel, 17 parts of filler, 1 part of sulfur, and activator 2 parts, 2 parts of plasticizer, 2 parts of anti-aging agent, 4 parts of organic foaming agent, 22 parts of paraffin oil.

[0101] The EPDM rubber is ethylidene norbornene type EPDM rubber.

[0102] The silica airgel is (methoxycarbonylaminomethyl) trimethoxysilane coupling agent modified silica airgel.

[0103] The preparation method of the (methoxycarbonylaminomethyl)trimethoxysilane coupling agent-modified silica airgel is the same as in Example 1.

[0104] The filler is dicarboxymethyl dithiocarbamate modified light calcium carbonate.

[0105] The preparation method of described dicarboxymethyl dithiocarbamate modified light calcium carbonate is with embodiment 1.

[0106] The activator is zinc oxide.

[0107] Describ...

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Abstract

The invention relates to the field of rubber, and particularly discloses a sound-insulation heat-preservation rubber product and a preparation method thereof. The formula comprises at least the following components: an ethylene-propylene-diene monomer, silicon dioxide aerogel, a filler, sulfur, an activator, a plasticizer, an anti-aging agent, an organic foaming agent and paraffin oil. According to the rubber product and method provided by the invention, the modified silicon dioxide aerogel is used, so that mechanical properties of silicon dioxide aerogel are improved, and mechanical properties and vulcanization properties of a rubber compound are further improved by controlling a usage amount ratio of the silicon dioxide aerogel; in addition, filler light weight calcium carbonate is modified, so that dispersibility of light weight calcium carbonate is improved, the vulcanization properties of the rubber compound are improved; and the modified silicon dioxide aerogel and the modified light weight calcium carbonate are comprehensively coordinated, so that the prepared rubber product has more excellent tensile strength, elongation at break and vulcanization properties.

Description

technical field [0001] The invention relates to the field of rubber, in particular to a sound-insulating and heat-insulating rubber product and a preparation method thereof. Background technique [0002] Ethylene-propylene rubber is a synthetic rubber formed by copolymerization of ethylene and propylene-based monomers, and its use and consumption are still expanding. According to the composition of monomer units in the rubber molecular chain, it can be divided into binary ethylene-propylene rubber and tertiary ethylene-propylene rubber. The former is a copolymer of ethylene and propylene; the latter is the third unit of ethylene, propylene and a small amount of non-conjugated dienes. Body copolymers, collectively referred to as ethylene-propylene rubber. Ethylene-propylene rubber is mainly used in the automobile industry, wire and cable industry, construction industry, etc., as well as civilian rubber products, waterproof materials and other rubber-plastic materials, such a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L23/16C08K9/06C08K7/26C08K9/04C08K3/26C08J9/10
CPCC08J9/102C08J9/105C08J9/009C08J9/0066C08J2203/04C08J2323/16
Inventor 张媛婷
Owner 南京大毛牛环保科技有限公司
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