Cationic ultra-fine and high-density fibers capable of being dyed at room temperature
A cationic, thin and high technology, applied in fiber processing, fiber chemical characteristics, filament generation and other directions, can solve the problems of high weaving cost, difficult to achieve mass production, difficult dyeing, etc., to enhance the interface bonding strength, improve the interface phase. Capacitive, ensure the effect of chemical properties
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Embodiment 1
[0025] The preparation method of the cationic room temperature dyeable superfine high-density fiber of this embodiment comprises the following steps:
[0026] 1) Add aliphatic and its derivatives and nano ZnO in a molar ratio of 1:1.3 into a reaction vessel, heat in a water bath to 60°C, and dry at 150°C;
[0027] 2) Then take aromatic dihydric alcohol and its derivatives, absolute ethanol, luminous powder, and zinc manganate and add them to the slurry kettle for beating; transport the slurry and the materials obtained in step 1) to the reaction kettle, and set up the reaction kettle. The temperature of the kettle is 230°C, and the reaction takes 11 minutes;
[0028] 3) Spraying the slurry obtained in step 2) on the surface of the ultra-fine high-density fiber melt to obtain modified ultra-fine high-density fiber A, which is then transported to the spinning device;
[0029] 4) Then terephthalic acid, ethylene glycol and carboxylic acid compounds, phenolic resin, and cetyltrim...
Embodiment 2
[0034] The preparation method of the cationic room temperature dyeable superfine high-density fiber of this embodiment comprises the following steps:
[0035] 1) Add aliphatic and its derivatives and nano-ZnO in a molar ratio of 1:1.2 into the reaction vessel, heat in a water bath to 70°C, and dry at 130°C;
[0036] 2) Then take aromatic dihydric alcohol and its derivatives, absolute ethanol, luminous powder, and zinc manganate and add them to the slurry kettle for beating; transport the slurry and the materials obtained in step 1) to the reaction kettle, and set up the reaction kettle. The temperature of the kettle is 235°C, and the reaction is 15 minutes;
[0037] 3) Spraying the slurry obtained in step 2) on the surface of the ultra-fine high-density fiber melt to obtain modified ultra-fine high-density fiber A, which is then transported to the spinning device;
[0038] 4) Then, magnetically stir terephthalic acid, ethylene glycol, carboxylic acid compounds, phenolic resin...
Embodiment 3
[0043] The preparation method of the cationic room temperature dyeable superfine high-density fiber of this embodiment comprises the following steps:
[0044]1) Add aliphatic and its derivatives and nano-ZnO in a molar ratio of 1:1.2 into a reaction vessel, heat in a water bath to 80°C, and dry at 120°C;
[0045] 2) Then take aromatic dihydric alcohol and its derivatives, absolute ethanol, luminous powder, and zinc manganate and add them to the slurry kettle for beating; transport the slurry and the materials obtained in step 1) to the reaction kettle, and set up the reaction kettle. The temperature of the kettle is 240°C, and the reaction time is 12 minutes;
[0046] 3) Spraying the slurry obtained in step 2) on the surface of the ultra-fine high-density fiber melt to obtain modified ultra-fine high-density fiber A, which is then transported to the spinning device;
[0047] 4) Then terephthalic acid, ethylene glycol and carboxylic acid compounds, phenolic resin, and cetyltri...
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