A kind of methanol to propylene device and method
A technology for producing propylene and methanol from methanol, applied in chemical instruments and methods, ether preparation, sustainable manufacturing/processing, etc., can solve the problems of increasing C4 cycle energy consumption and heater load, affecting propylene yield, and olefin waste, etc. Achieving the effects of efficient temperature control and stability, reduction of flying temperature and high propylene yield
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Embodiment 1
[0060] use as figure 1 Experiments are carried out in the simulated device shown, wherein the catalyst in the first reactor 101 (i.e. DME reactor) is γ-Al 2 o 3 (Select the DME-1 catalyst of Clariant Co., Ltd.), and fill in two layers. The second reactor 102 is provided with five layers of catalyst beds 9, and the catalysts are evenly packed into the first to fifth catalyst beds of the second reactor 102, wherein the distance between the catalyst beds is from the upper right to The lower gradually increases (the distance between any intermediate catalyst bed and the adjacent catalyst bed below it is 1.1 times the distance between the adjacent catalyst bed above it).
[0061]Wherein, the feed amount of fresh methanol to the first reactor 101 is 2.5kg / h, and the total amount of catalyst loaded in the first reactor is 1.8kg, and the reaction pressure is 0.8MPa. After the fresh methanol accounting for 60wt% of the total amount is preheated to about 270°C, it enters from the top...
Embodiment 2
[0065] The difference from Example 1 is that in the first product stream obtained, the first product stream accounting for (10±1)wt% is transported through the second feed pipe 4, and the first product flow accounting for (57±1)wt% The first product stream is conveyed through the third conveying pipe 3 and the remainder is conveyed through the first conveying pipe 5 . The temperature of the liquid phase from the separation column 107 is further controlled at 55±2°C. At the same time, the distance between any intermediate catalyst bed in the second reactor 102 and the adjacent catalyst bed below it is 1.2 times the distance between the adjacent catalyst bed above it. The experimental results are shown in Table 1.
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