Micro-fluidic liquid sample cell for dynamic spectral detection analysis and application thereof
A liquid sample, dynamic spectrum technology, applied in the measurement of color/spectral characteristics, material analysis by optical means, analysis of materials, etc. The effect of repeating the measurement many times, expanding the scope of application, and avoiding contamination of the sample
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Embodiment 1
[0050] Combine below Figure 1-Figure 4 and examples describe in detail the specific implementation of the present invention, such as Figure 1-Figure 4 As shown, this embodiment provides a microflow liquid sample cell for dynamic spectrum detection and analysis, which includes a magnetic induction rotation system, a motor drive and control system, and a sample cell system;
[0051] The sample pool system includes a sample pool 1;
[0052] The magnetic induction rotation system includes a rotor 4, a magnetic turntable 12 and a magnetic shaft 13; the rotor 4 is placed in the sample pool 1; the magnetic turntable 12 is used to control the rotation of the rotor 4 placed in the sample pool 1;
[0053] Described motor transmission and control system comprises power supply 28, controller 29 and DC motor 18; Described power supply 28 is electrically connected with controller 29 and DC motor 18; Described controller 29 is used for controlling the rotating speed of DC motor 18;
[00...
Embodiment 2
[0071] The micro-flow liquid sample cell described in Example 1 can be used in a femtosecond broadband pump (pump)-detection (probe) spectrometer system, and can perform chemical reaction kinetics at the macroscopic and single-molecule level of condensed phase complex molecules multiple studies.
[0072] The sample detected by the microfluidic liquid sample cell used in this embodiment is diethylaminohydroxyflavone (4'-N,N-diethylamino-3-hydroxyflavone, DEAHF).
[0073] In this example application, the shape of the sample cell is cuboid, the size of the sample cell is 1mm (width)×10mm (height)×45mm (length), the volume is less than 0.5ml, and the applicable wavelength is 200-2500nm. The width of the sample cell is actually the distance that light passes through the sample cell, that is, the optical path of the sample cell.
[0074] Figure 5 For the diethylaminohydroxyflavone femtosecond broadband pump-detection transient absorption spectrum shown in embodiment 2 and the mul...
Embodiment 3
[0078] The microflow liquid sample cell described in embodiment 1 can also be used in this more complicated device of femtosecond stimulated Raman spectrometer (results such as Figure 7 shown), and achieved good results.
[0079] In this example application, the shape of the sample cell is cuboid, the size of the sample cell is 1mm (width)×10mm (height)×45mm (length), the volume is less than 0.5ml, and the applicable wavelength is 200-2500nm. The width of the sample cell is actually the distance that light passes through the sample cell, that is, the optical path of the sample cell.
[0080] Figure 7 It is the real-time acquisition interface diagram of the femtosecond stimulated Raman spectrum shown in Example 3. Such as Figure 7 As shown, it can be seen that the stimulated Raman signal collected by the microfluidic liquid sample cell system can also maintain high stability and sensitivity for scarce and precious trace samples, which provides a good guarantee for subsequ...
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