Whitening and moisturizing facial mask essence containing roselle extract and preparation method of whitening and moisturizing mask essence
A technology of extract and roselle, which is applied in the field of whitening and moisturizing mask essence and its preparation, achieves the effect of wide source, beautiful color and accelerated tissue cell renewal
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Embodiment 1
[0019] A preparation method for whitening and moisturizing mask essence containing roselle extract, comprising the following steps:
[0020] (1) Weigh 50 g of roselle calyx superfine powder (average particle size ≤ 25 μm), add 500 mL of 50% ethanol solution, extract at room temperature for 6-8 h, take out the supernatant after centrifugation, and add 500 mL of 50% ethanol solution Extract again for 6-8 hours, combine the extracts and filter through a 200-mesh screen, concentrate under reduced pressure at 50°C in a rotary evaporator until there is no ethanol, and absorb with a macroporous resin column. After the adsorption is completed, use 80% ethanol solution to absorb The anthocyanins were eluted, and the eluate was collected and evaporated at 50°C until ethanol-free to obtain a concentrated solution of 220 mL roselle anthocyanin extract. Add 2.2 g disodium stannous citrate, stir and dissolve, and obtain a raw material solution a.
[0021] (2) Accurately weigh 15 g of rhodi...
Embodiment 2
[0027] A preparation method for whitening and moisturizing mask essence containing roselle extract, comprising the following steps:
[0028] (1) Weigh 500 g of roselle calyx superfine powder (average particle size ≤ 25 μm), add 5 L of 50% ethanol solution, extract at room temperature for 6-8 h, take out the supernatant after centrifugation, and add 5 L of 50% ethanol solution Extract again for 6-8 hours, combine the extracts and filter them through a 200-mesh sieve, concentrate under reduced pressure in a rotary evaporator at 50°C until there is no ethanol, and absorb with a macroporous resin column. After the adsorption is completed, use 80% ethanol solution to absorb The anthocyanins were eluted, and the eluate was collected and evaporated at 50°C until ethanol-free to obtain a concentrated solution of 2.5 L roselle anthocyanin extract. Add 25 g disodium stannous citrate, stir and dissolve, and obtain a raw material solution a.
[0029] (2) Accurately weigh 150 g of rhodiol...
Embodiment 3
[0035] A preparation method for whitening and moisturizing mask essence containing roselle extract, comprising the following steps:
[0036] (1) Weigh 2.5 kg roselle calyx superfine powder (average particle size ≤ 25 μm), feed it into a multi-functional dynamic extraction tank, add 50% ethanol solution in batches according to the ratio of solid to liquid 1:20, stir and extract at room temperature After 4 hours, filter to obtain about 47L of extract, concentrate under reduced pressure in a vacuum concentrator until there is no ethanol, load the sample on the macroporous resin column unit, and after the adsorption is completed, use 80% ethanol solution to remove the anthocyanins adsorbed on the resin column After elution, the collected eluent was concentrated under reduced pressure until there was no ethanol to obtain 8 L of concentrated solution of roselle anthocyanin extract, and 80 g of disodium stannous citrate was added, stirred and dissolved, and obtained as raw material so...
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