Oxynitride glass and production method thereof
A technology of oxynitride glass and production method, which is applied in glass furnace equipment, glass manufacturing equipment, manufacturing tools, etc., can solve the problems of unfavorable large-scale testing and production, high melting temperature, high price, etc., and achieve low temperature viscosity, The effect of reducing the melting temperature and making the preparation process safe
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Embodiment 1
[0023] This example provides a method for preparing oxynitride glass with a corundum crucible, comprising the following steps:
[0024] Chemical composition of oxynitride glass: SiO 2 46wt% Al 2 o 3 22.5wt% Y 2 o 3 17.6wt% CaO 11.7wt% AlN2.2wt%.
[0025] Specific steps: (1) Calculate by mass percentage, then accurately weigh and put it into a corundum mortar for grinding, mix evenly and pass through a 100-mesh sieve (2) After grinding, pour the powder into a corundum crucible, and put the corundum crucible into the atmosphere Furnace (3) closes the atmosphere furnace and rushes into nitrogen after vacuumizing, so repeat 3 times. During the melting process, the air pressure in the furnace is always maintained at 0.1-0.12Mpa, and the temperature reaches 300 degrees Celsius to pass cooling water. (4) Melting and holding at 1500°C for 2 hours and then cooling with the furnace, (5) Waiting for the furnace to drop to 650°C, holding for two hours for annealing. (6) After th...
Embodiment 2
[0027] This example provides a method for preparing oxynitride glass with a corundum crucible, comprising the following steps:
[0028] Chemical composition of oxynitride glass: SiO 2 41.4wt% Al 2 o 3 13.1 wt% Y 2 o 3 15.9 wt% CaO 10.5 wt% AlN 2.0 wt% ZnO 17.1 wt%.
[0029] Specific steps: (1) Calculate by mass percentage, then accurately weigh and put it into a corundum mortar for grinding, mix evenly and pass through a 100-mesh sieve (2) After grinding, pour the powder into a corundum crucible, and put the corundum crucible into the atmosphere Furnace (3) closes the atmosphere furnace and rushes into nitrogen after vacuumizing, so repeat 3 times. During the melting process, the air pressure in the furnace is always maintained at 0.1-0.12Mpa, and the temperature reaches 300 degrees Celsius to pass cooling water. (4) Melting and holding at 1480°C for 2 hours and then cooling with the furnace, (5) Waiting for the furnace to drop to 630°C, holding for 2 hours for anneal...
Embodiment 3
[0031] This example provides a method for preparing oxynitride glass with a corundum crucible, comprising the following steps:
[0032] Chemical composition of oxynitride glass: SiO 2 41.6wt%Al 2 o 3 10.8wt%Y 2 o 3 15.9 wt% CaO 10.6 wt% AlN 3.9 wt% ZnO 17.2 wt%.
[0033] Specific steps: (1) Calculate by mass percentage, then accurately weigh and put it into a corundum mortar for grinding, mix evenly and pass through a 100-mesh sieve (2) After grinding, pour the powder into a corundum crucible, and put the corundum crucible into the atmosphere Furnace (3) closes the atmosphere furnace and rushes into nitrogen after vacuumizing, so repeat 3 times. During the melting process, the air pressure in the furnace is always maintained at 0.1-0.12Mpa, and the temperature reaches 300 degrees Celsius to pass cooling water. (4) Melting and holding at 1480°C for 2 hours and then cooling with the furnace, (5) Waiting for the furnace to drop to 630°C, holding for two hours for anneali...
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