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A kind of preparation method of superhydrophobic coating and film with hydrophobic migration

A super-hydrophobic coating and hydrophobic migration technology, which is applied in the direction of antifouling/underwater coatings, coatings, paints containing biocide, etc., can solve the problems of not having hydrophobic migration and achieve excellent hydrophobic migration , Ease of large-scale production and coating, simple operation process

Active Publication Date: 2021-01-15
武汉疏能新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The super-hydrophobic anti-fouling flash one-component adhesive in this patent does not have the hydrophobic migration similar to RTV materials

Method used

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  • A kind of preparation method of superhydrophobic coating and film with hydrophobic migration
  • A kind of preparation method of superhydrophobic coating and film with hydrophobic migration
  • A kind of preparation method of superhydrophobic coating and film with hydrophobic migration

Examples

Experimental program
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Effect test

Embodiment 1

[0032] The embodiment of the present invention provides a method for preparing a superhydrophobic coating with hydrophobic mobility, comprising the following steps:

[0033] (1) adding concentrated ammonia water and tetraethyl orthosilicate to the ethanol solvent, stirring and aging, and then adding hexamethyldisilazane to prepare a superhydrophobic coating;

[0034] (2) In the super-hydrophobic coating prepared above, add silicone oil and a silane coupling agent with hydrophobic mobility to prepare a super-hydrophobic coating with hydrophobic migration.

[0035] Silicone oils include methyl silicone oil, ethyl silicone oil, methyl phenyl silicone oil, methyl chlorophenyl silicone oil, methyl ethoxy silicone oil, hydroxyl hydrogen silicone oil, methyl trifluoropropyl silicone oil, phenyl silicone oil, methyl One or more of hydrogen silicone oil, methyl vinyl silicone oil, ethyl hydrogen silicone oil, and methyl hydroxy silicone oil. The mass ratio of the silicone oil to the s...

Embodiment 2

[0038] The embodiment of the present invention provides a method for preparing a superhydrophobic coating with hydrophobic mobility, comprising the following steps:

[0039] In the super-hydrophobic coating, silicone oil with hydrophobic migration and silane coupling agent are added to prepare super-hydrophobic coating with hydrophobic migration. Superhydrophobic coatings without silicone oil can be purchased through online shopping and other channels, such as SM-supercoat-SHFC3150 produced by Shangmeng Technology (Zhangjiagang) Co., Ltd., which is made of nano-materials such as silicon oxide and montmorillonite and modified high-performance fluorocarbons Resin composition; "CCP002&CCP003- Super-hydrophobic and super-oleophobic nano-coating "normal temperature self-drying super-hydrophobic coating; NC317 super-hydrophobic coating produced by Changzhou Naroco Coatings Co., Ltd.

[0040] Silicone oils include methyl silicone oil, ethyl silicone oil, methyl phenyl silicone oil, m...

Embodiment 3

[0043] An embodiment of the present invention provides a method for preparing a superhydrophobic insulating film with hydrophobic mobility, comprising the following steps:

[0044] (1) Hydrophobic SiO 2 Preparation of nanoparticles: add 8mL concentrated ammonia water to 100mL ethanol and heat up to 40°C, then add 18mL tetraethylorthosilicate, stir for 1.5h, cool down, age for 24h, then add 20mL hexamethyldisilazane, Stir for 4 hours to obtain the superhydrophobic coating.

[0045] (2) In the state of stirring, add 0.3 g of polydimethylsilicone oil and 0.1 g of silane coupling agent (KH560) to the superhydrophobic coating prepared in step (1) to obtain a superhydrophobic coating with hydrophobic mobility .

[0046] (3) Spraying and curing the superhydrophobic coating prepared in step (2) on a glass substrate and drying naturally to obtain a superhydrophobic insulating film with hydrophobic mobility.

[0047] The embodiment of the present invention also provides a super-hydro...

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Abstract

The invention discloses a method for preparing a superhydrophobic coating and a film with a hydrophobic migration property, and relates to the technical field of hydrophobic materials. A method of introducing silicone oil having a migration property into the superhydrophobic coating is adopted, and the superhydrophobic coating has hydrophobic migration characteristics under the conditions that a superhydrophobic function of the original superhydrophobic coating is not weakened. The superhydrophobic insulating film formed by coating and curing of the superhydrophobic coating with the hydrophobic migration property has a 167-degree static state hydrophobic angle with water, and a roll angle can be as low as 1.6 degrees; hydrophilic diatomaceous earth is adopted on the surface of the film forsmearing, the static contact angle between the surface of the diatomaceous earth and the water is 151.2 degrees in 72 h, and the roll angle is 7.2 degrees, showing excellent hydrophobic migration. The product has great application value in the fields of self-cleaning anti-pollution flashover, electric anti-condensation, anti-icing and the like of high-voltage insulators.

Description

technical field [0001] The invention relates to the technical field of hydrophobic materials, in particular to a method for preparing a superhydrophobic coating and a film with hydrophobic mobility. Background technique [0002] Superhydrophobic film refers to a film with a contact angle of more than 150 degrees to water droplets and a roll angle of less than 10 degrees. It has functions such as waterproof, self-cleaning, and anti-fouling, so it has broad application prospects in daily life and industrial fields. The bionic superhydrophobic surface utilizes the bionic superhydrophobic self-cleaning principle of lotus leaves and cicada wings, etc., by modifying low surface energy components on the surface with micro-nano rough structure or constructing roughness on the surface of low surface energy, to realize the self-cleaning of solid surface. Super hydrophobic function. Due to the superhydrophobic properties, the water droplets take away the dust particles and dirt adheri...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D183/04C09D183/05C09D183/06C09D183/08C09D5/25C09D5/16C09D7/61C09D7/63
CPCC09D5/00C09D5/1675C09D5/1687C09D183/04C09D183/06C09D183/08C08K13/02C08K5/5415C08K5/544C08K3/28C08K5/5425C08K5/5435
Inventor 魏长伟
Owner 武汉疏能新材料有限公司
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