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A detection method for fluid flow state in overflow pipe of multi-layer fluidized bed

A multi-layer fluidized bed and fluid flow technology, which is applied in the directions of measuring devices, geophysical measurements, and processing detection response signals, can solve problems such as signal distortion, difficult maintenance, and easy blockage of pressure monitoring, and achieve timely response, high precision effect

Active Publication Date: 2021-01-01
ZHEJIANG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] 1) The pressure monitoring is easy to be blocked during the monitoring process, and it is difficult to maintain
[0008] 2) Both pressure pulsation monitoring and capacitance monitoring are plug-in, and holes must be drilled on the wall of the fluidized bed during installation. certain influence
[0009] 3) The environmental requirements are relatively high. For relatively harsh factory environments, such as high temperature, high pressure, dust and other environments, signal distortion may be caused, and the dynamic information of the fluid in the fluidized bed overflow pipe cannot be truly reflected.

Method used

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  • A detection method for fluid flow state in overflow pipe of multi-layer fluidized bed
  • A detection method for fluid flow state in overflow pipe of multi-layer fluidized bed
  • A detection method for fluid flow state in overflow pipe of multi-layer fluidized bed

Examples

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Embodiment example 1

[0037] In a gas-solid fluidized bed made of plexiglass with a height of 1000mm and an inner diameter of 150mm, the distribution plate is a porous plate, the aperture is 2.0mm, and the porosity is 2.6%. Air is used as the fluidizing gas, and the average particle size is 613.7μm. Polypropylene granules were used as fluidized granules. The acoustic emission probe model used is AE144S, the passive acoustic emission transducer is attached to the overflow pipe of the distribution plate, and the sampling frequency is 900kHz. Using the db2 wavelet function, the collected signal is decomposed by 10-scale wavelet, and the spectrum structure of the signal is characterized by the distribution of wavelet energy fractions in each scale. In the power spectrum of the particle-wall friction signal, there is mainly a peak with a main frequency of 25 kHz, and in the PSD of the particle-wall impact signal, there is mainly a peak with a main frequency of 90 kHz. Change different air speeds and ob...

Embodiment example 2

[0039] In a gas-solid fluidized bed made of plexiglass with a height of 1000mm and an inner diameter of 150mm, the distribution plate is a porous plate, the aperture is 2.0mm, and the porosity is 2.6%. Air is used as the fluidizing gas and the average particle size is 35.76μm. Pulverized coal particles are used as fluidized particles. The model of the acoustic emission probe used is PXR15, the passive acoustic emission transducer is attached to the overflow pipe of the distribution plate, and the sampling frequency is 600kHz. Change different air speeds and observe that the frequency in the acoustic signal is f collision =150-300kHz and f friction =18.75-37.5kHz energy fraction, to distinguish the feeding state of the fluidized bed overflow pipe. if D collision / D friction >3, indicating that the interaction between particles and the wall is dominant, the overflow pipe is not normally fed, and the power spectrum of the interaction between particles and the wall in the abno...

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Abstract

The invention discloses an acoustic detection method of a blanking state of a multi-layer fluidized bed reactor overflow pipe. An acoustic emission signal at the multi-layer fluidized bed reactor overflow pipe is received; the received acoustic emission signal is analyzed, and energy fractions of friction and collision signals in the acoustic signals are observed to distinguish the blanking stateof the multi-layer fluidized bed reactor overflow pipe. When the multi-layer fluidized bed reactor overflow pipe performs normal blanking, particles are transmitted in a dense phase, a flow state is aplunger flow, and interaction between particles and a wall surface focuses on friction. Under this state, in the received acoustic signal, Dcollision / Dfriction<=3. When the multi-layer fluidized bedreactor overflow pipe performs non-normal blanking, air moves upwardly through overflow pipe, air speed is too large so as to prevent the solid particles from moving downwardly, even carry particles to rise. Under this state, particles are transmitted in a dilute phase, interaction between particles and a wall surface focuses on collision, and in the received acoustic signal, Dcollision / Dfriction>3. The method disclosed by the invention has the characteristics of sensitivity, security and environmental protection, simplicity and quickness, can timely and correctly perform on-line analysis andcontrols production data through analysis results.

Description

technical field [0001] The invention relates to the detection of the feeding state of the overflow pipe of a multilayer fluidized bed reactor, in particular to a detection method for the fluid flow state of the overflow pipe of a multilayer fluidized bed reactor. Background technique [0002] The multi-layer fluidized bed can establish concentration gradient and temperature gradient vertically along the bed height, and reduce the axial back-mixing of particles and gas in the fluidized bed. The redistribution of gas through the distribution plates of each layer can inhibit the coalescence and growth of bubbles, effectively reduce the diffusion resistance, and improve the heat transfer and mass transfer rates. Therefore, as an important way to strengthen fluidized operation, multi-layer fluidized bed has been applied in various scales in catalytic cracking, iron ore gas reduction, calcination and drying of particles, production of activated carbon and carbon nanotubes, ion exc...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N29/44G01V1/00
CPCG01N29/44G01V1/00
Inventor 孙婧元杨遥郭晓云林王旻黄正梁王靖岱阳永荣廖祖维蒋斌波叶健马玉龙郭高顺董轩
Owner ZHEJIANG UNIV
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