CdS/Cu2S/Co-based photoelectric catalytic material and preparation method thereof
A photoelectric catalysis and co-catalyst technology, applied in chemical instruments and methods, physical/chemical process catalysts, electrodes, etc., can solve the problems of low reserves, high cost, restricting large-scale practical application, etc., and achieve simple preparation process and stable improvement. The effect of stable, efficient and stable photoelectric catalytic water splitting performance
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Embodiment 1
[0054] A commercial 10 mm × 25 mm FTO conductive glass substrate was placed in piranha washing solution (98% H 2 SO 4 :30%H 2 o 2 =3:1) for 3 hours, ultrasonically washed with ultrapure water for 10 minutes, and dried in a drying oven.
[0055] Weigh 0.1603 grams of cadmium sulfate (3CdSO 4 ·8H 2 O), 0.8373 grams of thiourea (SC (NH 2 ) 2 ) into a 150 milliliter beaker, then add 50 milliliters of ultrapure water, stir for 5 minutes to dissolve the above-mentioned medicine completely, then add 8.5 milliliters of ammonia water, seal and continue to stir for 90 seconds. Quickly pour the above solution into a 100ml wide-mouth reagent bottle;
[0056] A 10 mm × 25 mm FTO conductive glass substrate is suspended and immersed in the solution of the above-mentioned wide-mouth reagent bottle with a thin wire, and the immersion area is 1 square centimeter, and the bottle mouth is sealed. Put it into a water bath and start heating. After the temperature of the water bath rises to ...
Embodiment 2
[0069] Place a commercial 20 mm × 30 mm FTO conductive glass substrate in piranha wash solution (98% H 2 SO 4 :30%H 2 o 2 =3:1) for 3 hours, ultrasonically washed with ultrapure water for 15 minutes, and dried in a vacuum oven.
[0070] Weigh 0.3207 grams of cadmium sulfate (3CdSO 4 .8H 2 O), 1.6746 grams of thiourea (SC (NH 2 ) 2 ) into a 250 milliliter beaker, then add 100 milliliters of ultrapure water, stir for 5 minutes to dissolve the above-mentioned medicines completely, then add 17 milliliters of ammonia water, seal, and continue to stir for 90 seconds. Quickly pour the above solution into a 200ml wide-mouth reagent bottle;
[0071] A 20 mm × 30 mm FTO conductive glass substrate is suspended and immersed in the solution of the above-mentioned wide-mouth reagent bottle with a thin wire, and the bottle mouth is sealed. Put it in a water bath and start heating. After the temperature of the water bath rises to 60°C, keep it at 60°C for 30 minutes; during this proce...
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