Temperature sensor and its preparation method
A technology of temperature sensor and carbon nanomaterials, applied in thermometers, instruments, thermometers with directly sensitive electrical/magnetic elements, etc., can solve the problem that the heat transfer balance model cannot accurately describe the measured object, and the temperature measuring element cannot The temperature measurement requirements and data acquisition board requirements are high, so that the processing methods can be automated, the design is flexible, and the material and process costs are low.
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Embodiment 1
[0052] Commercially available single-walled carbon nanotubes were used as temperature-sensitive materials. An aluminum sheet is used as the heat conduction substrate 1 with a thickness of 0.16 mm.
[0053] First, insulate the aluminum sheet, and modify a layer of polymer layer on the upper surface of the aluminum sheet. The specific method is as follows:
[0054] Spin-coat a polyamic acid solution with a mass fraction of 10% on the surface of the aluminum sheet. The spin-coating program is set to 1000 rpm for 30 s and 3000 rpm for 30 s. Heat the spin-coated aluminum plate at 100 °C for 5 min. , heated at 150°C for 5min to remove part of the solvent and form a polymer layer. Then, the temperature-sensitive carbon nanomaterial layer 2 composed of temperature-sensitive materials is compounded on the surface of the polymer layer, and the temperature-sensitive carbon nanomaterial layer 2 is a continuous structure (square), and the specific method is as follows:
[0055] At 160° C...
Embodiment 2
[0058] Commercially available graphite nanosheets were used as temperature-sensitive materials. The aluminum sheet is used as the heat conduction substrate with a thickness of 0.16mm.
[0059] First, insulate the aluminum sheet, and modify a layer of polymer layer on the upper surface of the aluminum sheet. The specific method is as follows:
[0060] Spin-coat a polyamic acid solution with a mass fraction of 10% on the surface of the aluminum sheet. The spin-coating program is set to 1000 rpm for 30 s and 3000 rpm for 30 s. Heat the spin-coated aluminum plate at 100 °C for 5 min. , heated at 150°C for 5min to remove part of the solvent and form a polymer layer. Then, on the surface of the polymer layer, a temperature-sensitive carbon nanomaterial layer composed of a temperature-sensitive material is compounded. The temperature-sensitive carbon nanomaterial layer is a continuous structure (square), and the specific method is as follows:
[0061] At 160°C, the aqueous solution...
Embodiment 3
[0063] Polyimide is used as a temperature-sensitive material to form a temperature-sensitive carbon nanomaterial layer with a continuous structure. The aluminum sheet is used as the heat conduction substrate. The preparation method of this implementation temperature sensor is as follows:
[0064] First, 1.5 g of precursor solution, which is N,N'-dimethylacetamide solution of polyamic acid, was spin-coated on a 0.16 mm thick aluminum sheet to form a polyamic acid-aluminum sheet composite matrix. Carry out heat treatment on the spin-coated polyamic acid-aluminum sheet composite substrate, specifically remove water at 100°C for 0.5h, then remove solvent at 150°C for 1.5h, and finally heat treat at 300°C to make polyamic acid amide into polyimide to form a polyimide-aluminum sheet composite matrix. Place the polyimide-aluminum sheet composite matrix in a laser cutting machine for laser scanning carbonization, the laser light source used is CO 2 Laser, the laser power is control...
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