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Three-shell iron-silicon-substrate soft magnet composite material and manufacturing method thereof

A soft magnetic composite material, three-shell technology, applied in the fields of inorganic material magnetism, metal processing equipment, transportation and packaging, etc., can solve the problems of high energy and raw material loss, complex preparation process, unfavorable mass preparation, etc., and achieve constant conductance. The effect of good magnetic properties, good chemical stability and good application prospects

Active Publication Date: 2018-11-13
WUHAN UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The insulating layer of the obtained soft magnetic composite material is relatively uniform, and the magnetic properties are good, but the preparation process is complicated, the operation is not easy, and the loss of energy and raw materials is large, which is not conducive to mass production.

Method used

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  • Three-shell iron-silicon-substrate soft magnet composite material and manufacturing method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] A three-shell iron-silicon-based soft magnetic composite material and a preparation method thereof. The steps of the preparation method described in this embodiment are:

[0034] The first step, composite powder preparation

[0035] According to the iron-silicon alloy powder:water mass ratio of 1:(5-40), the iron-silicon alloy powder is placed in the water, stirred at a water temperature of 30-60°C for 5-10 hours, and solid-liquid separation, A composite powder is obtained.

[0036] The second step, cold forming

[0037] The composite powder is vacuum-dried, loaded into a mold, and cold-pressed under the condition of 300-600 MPa to obtain a green body.

[0038] The third step, sintering

[0039] The green body is placed in a high-temperature sintering furnace, heated to 800-900° C. under vacuum conditions, and sintered for 0.5-1 hour to obtain a sintered green body.

[0040] The fourth step, heat treatment

[0041] The sintered green body is placed in a heat treat...

Embodiment 2

[0046] A three-shell iron-silicon-based soft magnetic composite material and a preparation method thereof. The steps of the preparation method described in this embodiment are:

[0047] The first step, composite powder preparation

[0048] According to the iron-silicon alloy powder:water mass ratio of 1:(20-55), the iron-silicon alloy powder is placed in the water, stirred at a water temperature of 35-65°C for 10-15 hours, and solid-liquid separation, A composite powder is obtained.

[0049] The second step, cold forming

[0050] The composite powder is vacuum-dried, loaded into a mold, and cold-pressed under the condition of 450-750 MPa to obtain a green body.

[0051] The third step, sintering

[0052] The green body is placed in a high-temperature sintering furnace, heated to 900-1000° C. under vacuum conditions, and sintered for 1.5-2 hours to obtain a sintered green body.

[0053] The fourth step, heat treatment

[0054] The sintered green body is placed in a heat tre...

Embodiment 3

[0059] A three-shell iron-silicon-based soft magnetic composite material and a preparation method thereof. The steps of the preparation method described in this embodiment are:

[0060] The first step, composite powder preparation

[0061] According to the iron-silicon alloy powder:water mass ratio of 1:(35-70), the iron-silicon alloy powder is placed in the water, stirred at a water temperature of 40-70°C for 15-20h, and solid-liquid separation, A composite powder is obtained.

[0062] The second step, cold forming

[0063] The composite powder is vacuum-dried, loaded into a mold, and cold-pressed under the condition of 600-900 MPa to obtain a green body.

[0064] The third step, sintering

[0065] The green body is placed in a high-temperature sintering furnace, heated to 1000-1100° C. under protective atmosphere conditions, and sintered for 2.5-3 hours to obtain a sintered green body.

[0066] The fourth step, heat treatment

[0067] The sintered green body is placed ...

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Abstract

The invention relates to a three-shell iron-silicon-substrate soft magnet composite material and a manufacturing method thereof. The technical scheme is characterized in that iron-silicon alloy powderis placed into water according to a iron-silicon alloy powder to water mass ratio of 1:(5-100); the mixture is stirred for 5-30 h at 30-80 DEG C; composite powder is obtained after solid-liquid separation; the composite powder is subjected to vacuum drying and placed in a mould; the powder is moulded through cold pressing under the condition of 300-1200 MPa to obtain a blank body; the blank bodyis placed in a high-temperature sintering furnace, is heated to 800-1300 DEG C at a vacuum condition or at a protection atmosphere condition, and is sintered for 0.5-5 h to obtain the sintered blank body; the sintered blank body is placed in a thermal treatment furnace, is heated to 500-1200 DEG C at the vacuum condition or the protection atmosphere condition and is subjected to thermal treatmentfor 0.5-5 h; and the blank body is furnace cooled to obtain the three-shell iron-silicon-substrate soft magnet composite material. The manufacturing method is simple in technique and low in productioncost; the manufactured product is not only uniform in isolation layer and extremely low in magnetic loss; and besides, the saturation flux density is high and constant magnetic permeability is high.

Description

technical field [0001] The invention belongs to the technical field of iron-silicon-based soft magnetic composite materials. In particular, it relates to a three-shell iron-silicon-based soft magnetic composite material and a preparation method thereof. Background technique [0002] FeSi-based soft magnetic composite materials are widely used in inverters, Electronic components such as inductors, transformers, and choke coils are involved in many fields such as motors, telecommunications, and power supplies. [0003] It is worth mentioning that as the frequency of use increases, the eddy current loss of soft magnetic composite materials increases exponentially, and the insulating coating of magnetic particles is undoubtedly the most effective way to reduce eddy current loss. On this basis, insulation coating is mainly divided into two types: organic coating and inorganic coating. The common organic coating method is to mix magnetic particles and organic coating materials ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F1/02B22F3/10B22F3/24H01F1/22
CPCH01F1/22B22F3/1007B22F3/24B22F2998/10B22F2999/00B22F2003/248B22F1/16B22F2201/20B22F2201/02B22F2201/11B22F3/02
Inventor 樊希安罗自贵李光强李亚伟
Owner WUHAN UNIV OF SCI & TECH
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