Visible light driven Cu2O@N-CNTs compound microsphere motor taking glucose as fuel and preparation method thereof
A technology of glucose and visible light, which is applied to the preparation of microspheres, microcapsule preparations, chemical instruments and methods, etc., can solve the problems that the operating environment of light-driven micro-nano motors is not safe and friendly, cannot meet practical applications, and cannot reach practical applications. , to achieve good environmental adaptability and dual regulation of movement, the preparation method is simple and easy, and the effect of improving conductivity
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Embodiment 1
[0034] A glucose-fueled and visible-light-driven Cu 2 The preparation method of O@N-CNTs composite microsphere motor comprises the following steps:
[0035] a) Take 0.3mg N-CNTs and disperse them into 2.5mL ethanol solution, and carry out ultrasonic dispersion treatment for 24 hours;
[0036] b) Dissolve 0.1g of copper acetate and 0.4g of sodium dodecylsulfonate in 8mL of water, add them to the ethanol dispersion solution in step a), and then add 5.5mL of ethanol;
[0037] c) heating the mixed solution obtained in step b) to 73°C in an oil bath;
[0038] d) Add 0.14g sodium hydroxide and 0.12g glucose, and react for about 30 minutes to obtain a brick red product;
[0039] e) The product was centrifuged and washed about 5 times with deionized water, and then dried in a vacuum oven at 60°C to obtain Cu 2 O@N-CNTs composite microsphere motor.
Embodiment 2
[0041] A glucose-fueled and visible-light-driven Cu 2 The preparation method of O@N-CNTs composite microsphere motor comprises the following steps:
[0042] a) Disperse 0.5mg of N-CNTs into 4.2mL of ethanol solution and perform ultrasonic dispersion treatment for 24 hours;
[0043] b) Dissolve 0.1g of copper acetate and 0.4g of sodium dodecylsulfonate in 8mL of water, add them to the ethanol dispersion solution in step a) respectively, and then add 3.8mL of ethanol;
[0044] c) heating the mixed solution obtained in step b) to 73°C in an oil bath;
[0045] d) Add 0.14g sodium hydroxide and 0.12g glucose, and react for about 30 minutes to obtain a brick red product;
[0046] e) The product was centrifuged and washed about 5 times with deionized water, and then dried in a vacuum oven at 60°C to obtain Cu 2 O@N-CNTs composite microsphere motor.
Embodiment 3
[0048] A glucose-fueled and visible-light-driven Cu 2 The preparation method of O@N-CNTs composite microsphere motor comprises the following steps:
[0049] a) Disperse 0.7mg of N-CNTs into 5.8mL of ethanol solution and perform ultrasonic dispersion treatment for 24 hours;
[0050] b) Dissolve 0.1g of copper acetate and 0.4g of sodium dodecylsulfonate in 8mL of water, add them to the ethanol dispersion solution in step a) respectively, and then add 2.2mL of ethanol;
[0051] c) heating the mixed solution obtained in step b) to 73°C in an oil bath;
[0052] d) Add 0.14g sodium hydroxide and 0.12g glucose, and react for about 30 minutes to obtain a brick red product;
[0053] e) The product was centrifuged and washed about 5 times with deionized water, and then dried in a vacuum oven at 60°C to obtain Cu 2 O@N-CNTs composite microsphere motor.
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