Multifunctional flame-retardant blanket and preparation method thereof
A multi-functional, flame-retardant acrylic fiber technology, used in blankets, wet spinning, man-made filaments made of viscose, etc., can solve the problems of poor comfort, easy generation of static electricity, melting and dripping of pure polyester flame-retardant blankets
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Embodiment 1
[0023] Embodiment 1: Preparation of SOL FR
[0024] 1. Synthesis of multi-element synergistic flame retardants
[0025] 1.1 Synthesis of DDPS (2,2'-oxobis(5,5-dimethyl-1,3,2-dioxaphosphine-2,2'-disulfide))
[0026] Molecular formula C 5 h 10 o 2 PS-O-SPO 2 h 10 C 5
[0027] first step
[0028] Phosphor trichloride 328kg, neopentyl glycol 202.3kg, solvent benzene 165L, heated to 40°C, stirred and dissolved completely. Slowly add 305kg of pyridine dropwise, control the temperature at 45-75°C, keep it warm for 2 hours, wash with pure water, filter, and dry. A white intermediate was obtained for use.
[0029] second step
[0030] Above-mentioned intermediate 364kg, solubilizer dioxane 155L, pure water 38.5kg, heating dissolves intermediate. Slowly add 143.5kg of pyridine dropwise, control the temperature at 85-100°C, keep the reaction for 2 hours, wash with pure water, filter, and dry. White needle-like crystals were obtained for use.
[0031] Grinding to prepare 20%...
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