Preparation method of iron, cobalt and nitrogen co-doped hierarchical pore carbon nanosheet oxygen reduction catalyst
A technology of graded porous carbon and nanosheets, which is applied in electrical components, battery electrodes, circuits, etc., to achieve the effect of simple preparation method and high oxygen reduction activity
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Embodiment 1
[0046] (1) Preparation of ZnO nanosheets
[0047] Add 55mL 0.02mol L to a 100mL Erlenmeyer flask –1 Zn(AC) 2 2H 2 O aqueous solution, under stirring, 5mL2mol L –1 Aqueous NaOH solution was added dropwise to the above solution, and after the dropwise addition was completed, it was stirred for 30 min, and a white precipitate was formed at room temperature. The mixture was then transferred to an autoclave and maintained at 150 °C for 3 h in an oven. After cooling to room temperature, ZnO nanosheets were obtained by centrifugation, washing, drying and crystallization.
[0048] (2) Preparation of core-shell structure ZnO@Zn / Fe / Co-ZIF precursor
[0049] Take step 1) 80.0 mg of ZnO nanosheets was added to an Erlenmeyer flask filled with a mixed solvent of DMF and water (64 mL, volume ratio 3:1), ultrasonicated for 20 min at room temperature to fully diffuse, and then 0.66 g of 2-methyl For imidazole, after ultrasonication for 5 minutes, add 20 mg of iron triacetylacetonate for...
Embodiment 2
[0055] (1) Preparation of ZnO nanosheets
[0056] Add 55mL 0.02mol L to a 100mL Erlenmeyer flask –1 Zn(AC) 2 2H 2 O aqueous solution, under stirring, 5mL2mol L –1 Aqueous NaOH solution was added dropwise to the above solution, and after the dropwise addition was completed, it was stirred for 30 min, and a white precipitate was formed at room temperature. The mixture was then transferred to an autoclave and maintained at 150 °C for 3 h in an oven. After cooling to room temperature, ZnO nanosheets were obtained by centrifugation, washing, drying and crystallization.
[0057] (2) Preparation of core-shell structure ZnO@Zn / Fe-ZIF precursor
[0058] Take step 1) 80.0 mg of ZnO nanosheets was added to an Erlenmeyer flask filled with a mixed solvent of DMF and water (64 mL, volume ratio 3:1), ultrasonicated for 20 min at room temperature to fully diffuse, and then 0.66 g of 2-methyl For imidazole, after ultrasonication for 5 minutes, add 20.0 mg of iron triacetylacetonate, mix...
Embodiment 3
[0064] (1) Preparation of ZnO nanosheets
[0065] Add 55mL 0.02mol L to a 100mL Erlenmeyer flask –1 Zn(AC) 2 2H 2 O aqueous solution, under stirring, 5mL2mol L –1 Aqueous NaOH solution was added dropwise to the above solution, and after the dropwise addition was completed, it was stirred for 30 min, and a white precipitate was formed at room temperature. The mixture was then transferred to an autoclave and maintained at 150 °C for 3 h in an oven. After cooling to room temperature, ZnO nanosheets were obtained by centrifugation, washing, drying and crystallization.
[0066] (2) Preparation of core-shell structure ZnO@Zn / Co-ZIF precursor
[0067] Take step 1) 80.0 mg of ZnO nanosheets was added to an Erlenmeyer flask filled with a mixed solvent of DMF and water (64 mL, volume ratio 3:1), ultrasonicated for 20 min at room temperature to fully diffuse, and then 0.66 g of 2-methyl Imidazole, after ultrasonication for 5 minutes, add 25.0 mg of cobalt nitrate hexahydrate, mix ...
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