Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

A detection cu 2+ Fluorescent probes, preparation methods, and preparation and use methods of fluorescent test strips

A technology of fluorescent probes and test strips, applied in fluorescence/phosphorescence, chemical instruments and methods, luminescent materials, etc., can solve the problem that metal ion identification is not specific, cannot achieve real-time on-site detection, and fluorescent test strips process. Complicated and cumbersome problems, to achieve the effect of low cost, rapid response and simple method

Inactive Publication Date: 2020-11-06
QIQIHAR UNIVERSITY
View PDF1 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] The present invention is to solve the existing laboratory traditional method to detect Cu 2+ Due to the limitation of the instrument and the high cost, the technical problem of real-time on-site detection cannot be achieved; the use of fluorescent probe method to detect Cu 2+ When the main body does not have specificity in the identification of metal ions, the technical problem of poor anti-interference ability; making Cu 2+ The process of fluorescent test paper is complex and cumbersome, and the technical problem is high cost

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A detection cu  <sup>2+</sup> Fluorescent probes, preparation methods, and preparation and use methods of fluorescent test strips
  • A detection cu  <sup>2+</sup> Fluorescent probes, preparation methods, and preparation and use methods of fluorescent test strips
  • A detection cu  <sup>2+</sup> Fluorescent probes, preparation methods, and preparation and use methods of fluorescent test strips

Examples

Experimental program
Comparison scheme
Effect test

specific Embodiment approach 1

[0027] Specific embodiment one: the detection of Cu in this embodiment 2+ The structural formula of the fluorescent probe is:

[0028]

specific Embodiment approach 2

[0029] Specific embodiment two: specific embodiment one is used for detecting Cu 2+ The preparation method of fluorescent probe is carried out according to the following steps:

[0030] One, according to the ratio of the substance of 2-(2-aminophenyl) phenanthroimidazole and pyridine-2-carbaldehyde is 1:(1~3), the 2-(2-aminophenyl) phenanthroimidazole Add pyridine-2-carbaldehyde into alcohol solvent, stir and react for 1-5 hours, and solids will precipitate out after the reaction;

[0031] 2. Suction filter the precipitated solid, then wash the filter cake with alcohol solvent and distilled water, collect the filter cake and dry it to obtain the crude product;

[0032] 3. Recrystallize the crude product with an organic solvent to obtain Cu 2+ fluorescent probes.

specific Embodiment approach 3

[0033] Embodiment 3: The difference between this embodiment and Embodiment 2 is that the alcohol solvent described in step 1 is methanol, ethanol, propanol, isopropanol or butanol; the others are the same as Embodiment 2.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention provides a Cu<2+> detection fluorescence probe, a preparation method of the Cu<2+> detection fluorescence probe, and a use method and preparation of a fluorescence test paper strip, relates to the Cu<2+> detection fluorescence probe, and the preparation method and the use method of the Cu<2+> detection fluorescence probe, and aims at solving the technical problems that the existing Cu<2+> detection cannot realize the field detection due to instrument limitation and higher cost; during the Cu<2+> detection by using a fluorescence probe method, the anti-interference capability of amain body on metal ions is poorer. The fluorescence probe has a structure formula shown in the description, and is prepared from 2-(2-aminophenyl)phenanthro-imidazole and pyridine-2-formaldehyde through reaction. The Cu<2+> detection fluorescence probe can be prepared into a solution; next, qualitative filter paper is sheared into strips to be soaked into the solution; after the drying, the fluorescence test paper strip for detecting the Cu<2+> can be obtained. Whether the sample contains Cu<2+> or not can be judged through watching whether the color of the test paper strip becomes bright light purple from the dark purple or not. The Cu<2+> detection fluorescence probe synthesis method is simple; the cost is low; the steps are simple; the yield is as high as 70 to 98 percent; the probe can be used for detecting the Cu<2+> in the water system environment.

Description

technical field [0001] The invention belongs to detecting Cu 2+ technical field involving the detection of Cu 2+ Preparation and Detection of Fluorescent Probes for Cu 2+ Preparation of fluorescent test strip and method of use thereof. Background technique [0002] Copper is an indispensable micronutrient element for human health. It is a constituent element of hemocyanin in the human body. It is very important for the development and function of the blood, central nervous system and immune system, hair, skin and bone tissue, as well as the brain, liver and heart. important influence. However, Cu present in excess 2+ It has adverse effects on organisms and the environment, such as maintaining metabolism in the human body, liver cirrhosis, liver ascites, etc., so Cu 2+ It is very important to carry out qualitative and quantitative detection. Traditional Cu 2+ Detection methods include ion plasma mass spectrometry, atomic absorption spectrometry, atomic emission spectro...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C07D401/12C09K11/06G01N21/64
CPCC07D401/12C09K11/06C09K2211/1044G01N21/643G01N2021/6439
Inventor 阚伟尹浩纯卜凡强赵冰何玉倩阚宏泽宋波荆涛
Owner QIQIHAR UNIVERSITY
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products