A kind of copper-doped carbon nano-coated fruit fresh-keeping agent and its preparation method and application
A copper-doped, carbon nanotechnology, applied in the direction of protecting fruits/vegetables with a protective coating, can solve the problems of high moisture absorption, low strength of fresh-keeping coating, poor antibacterial ability, etc., to reduce respiration and moisture. Loss of , the effect of preventing decay
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Embodiment 1
[0037] Embodiment 1: Nano-coated fruit fresh-keeping agent is used for citrus fresh-keeping
[0038] 1. Preparation of copper-doped carbon nanomaterials (Cu-CDs): 1.6-2.0gNa 2 [Cu(EDTA)] and 0.1-0.3g ascorbic acid, mixed evenly, placed in a corundum boat with a cover, roasted in a high-temperature tube furnace at 300°C for 2-3h, after the roasting was completed, the black product was ground and dissolved in 100mL deionized water, and ultrasonic 20-30min. Then the black suspension was centrifuged at 15000rpm for 15-20min, and the supernatant was passed through a 0.22μm filter membrane. The filtrate was taken and dried in a vacuum oven at 60° C. for 24 hours to obtain copper-doped carbon nanomaterials.
[0039] 2. Preparation of silver nanoparticles (AgNPs): Add 10-50mL (0.01mol / L) silver nitrate solution to a 25mL round-bottomed flask equipped with magnetons, then add 10-50mL (0.5mol / L) polyvinylpyrrolidone (PVP ), after stirring in an ice-water bath, add 15-50mL (0.01mol / L)...
Embodiment 2
[0056] Embodiment 2: Nano-coated fruit preservative is used for litchi preservation
[0057] 1. Preparation of copper-doped carbon nanomaterials (Cu-CDs): same as Example 1.
[0058] 2. Preparation of nano-silver (AgNPs): same as Example 1.
[0059] 3. Preparation of copper-doped carbon nano-coating preservative (Cu-CDs-TM): same as in Example 1.
[0060] 4. Preparation of antistaling agent (TM) without copper-doped carbon nano-coating: same as in Example 1.
[0061] 5, litchi preservation experiment: with embodiment 1.
[0062] (1) Effect of nano-coating film on sensory indicators of litchi
[0063] The lychees shown in Table 4 were subjected to sensory analysis. By comparing the sensory indicators such as appearance, pulp, color and flavor of lychees, the fresh-keeping effect of the coating film treatment group was better than that of the blank group, and the fresh-keeping effect of the Cu-CDs-TM coating film Good, 7d storage still has food value. Because after the frui...
Embodiment 3
[0074] Embodiment 3: Nano-coated fruit fresh-keeping agent is used for mango fresh-keeping
[0075] 1. Preparation of copper-doped carbon nanomaterials (Cu-CDs): same as Example 1.
[0076] 2. Preparation of nano-silver (AgNPs): same as Example 1.
[0077] 3. Preparation of copper-doped carbon nano-coating preservative (Cu-CDs-TM): same as in Example 1.
[0078] 4. Preparation of antistaling agent (TM) without copper-doped carbon nano-coating: same as in Example 1.
[0079] 5. Mango preservation experiment: with embodiment 1.
[0080] (1) Effect of nano-coating film on sensory indicators of mango
[0081] The mangoes shown in Table 7 were subjected to sensory analysis, the mangoes in the blank group matured quickly, and the mangoes were fully mature on the 8th day, and the flavor decreased significantly on the 12th day, indicating that the pulp water loss was serious, sugar substances were decomposed, and the mangoes were gradually aging; after TM and More than half of the...
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Abstract
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