Acrylate emulsion for plastic base materials and method for preparing acrylate emulsion
A technology of methyl methacrylate and acrylate, which is applied in the field of acrylate emulsion of plastic substrates and its preparation, can solve the problems of poor adhesion of plastic substrates, poor solvent resistance, and poor paint mixing stability, etc., and achieve good Tolerance of paint blending, improvement of gloss fullness, and effect of improving adhesion
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[0041] In addition, the present invention also provides a method for preparing the acrylate emulsion for plastic substrates, specifically comprising the following steps:
[0042] a) Preparation of bottom material liquid A: In the reaction kettle equipped with agitator, condenser and constant flow pump feeding device, add 10-30 parts of deionized water and 0.5-1 part of surfactant, and raise the temperature in the kettle to to 80-85°C;
[0043] b) Preparation of monomer solution B: butyl acrylate, methyl methacrylate, styrene, functional monomer, remaining surfactant, hydrophilic unsaturated organic acid 0.5- 2 parts, 5-10 parts of deionized water, mixed into a uniform solution, and stirred for 20-30 minutes for later use;
[0044] c) Preparation of initiator solution C: add the initiator of the formula amount into the remaining deionized water, stir and dissolve for subsequent use;
[0045] d) When the temperature in the kettle reaches 80-85°C, add 1-5 parts of the monomer s...
Embodiment 1
[0050] A kind of acrylate emulsion for plastic substrate, by weight, the acrylate emulsion comprises the following raw materials: 40 parts of deionized water, 10 parts of butyl acrylate, 25 parts of methyl methacrylate, 5 parts of styrene, 2 parts of hydrophilic unsaturated organic acid, 1 part of functional monomer, 1 part of surfactant, 0.1 part of initiator, and 1.5 parts of pH regulator.
[0051] The hydrophilic unsaturated organic acid is a mixed solution of 1 part of acrylic acid and 1 part of methacrylic acid.
[0052] The functional monomer is vinyltrimethoxysilane.
[0053] The surfactant is a combined emulsifier formed by mixing an anionic emulsifier and a nonionic emulsifier at a mass ratio of 1:1. The anionic emulsifier uses sodium dodecylsulfonate; the nonionic emulsifier uses alkylphenol polyoxyethylene ether.
[0054] The initiator is ammonium persulfate.
[0055] The pH regulator is ammonia water.
[0056] In addition, the present invention also provides a ...
Embodiment 2
[0065] A kind of acrylate emulsion for plastic substrate, by weight, the acrylate emulsion comprises the following raw materials: 45 parts of deionized water, 12 parts of butyl acrylate, 28 parts of methyl methacrylate, 7 parts of styrene, 2.5 parts of hydrophilic unsaturated organic acid, 1.5 parts of functional monomer, 1.5 parts of surfactant, 0.3 part of initiator, and 3 parts of pH regulator.
[0066] The hydrophilic unsaturated organic acid is mixed with acrylic acid and methacrylic acid at a ratio of 4:1.
[0067] The functional monomer is mixed with vinyltrimethoxysilane and methacryloxypropyltrimethoxysilane in a ratio of 2:1.
[0068] The surfactant is a combined emulsifier formed by mixing an anionic emulsifier and a nonionic emulsifier at a mass ratio of 2:1. The anionic emulsifier adopts sodium dialkyl-2-sulfosuccinate; the nonionic emulsifier adopts polyoxyethylene sorbitan monooleate.
[0069] The initiator is potassium persulfate.
[0070] The pH regulator i...
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