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Preparation method of humic acid suspended liquid fertilizer

A liquid fertilizer, humic acid technology, applied in the preparation of organic fertilizers, liquid fertilizers, nitrate fertilizers, etc., can solve the problems of poor stability of suspended fertilizers, poor adhesion of crop leaves, and low content, and achieve fluidity. The effect of improving and reducing affinity and improving dispersion performance

Inactive Publication Date: 2018-09-07
吴刚
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The technical problem mainly solved by the present invention is that the content of active ingredients such as nitrogen, phosphorus, and potassium in the existing humic acid-containing liquid fertilizers is generally low, and precipitation is easy to affect crop absorption, and the existing suspension-type liquid fertilizers are stable. Poor, the suspension fertilizer has poor adhesion to the crop leaf surface, and is easily washed away by rain. A method for preparing a humic acid-based suspension liquid fertilizer is provided.

Method used

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  • Preparation method of humic acid suspended liquid fertilizer

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Embodiment Construction

[0024]Take the sweet potato starch wastewater from the starch factory and the secondary sedimentation activated sludge and mix them according to the mass ratio of 5:1 to obtain the suspended sludge. After adjusting the pH of the suspended sludge to 9.8-10.2 with a sodium hydroxide solution with a mass fraction of 15%, Place it in a high-pressure steam pot for 50-60 minutes, control the temperature of the high-pressure steam pot to 120-150 ° C, and the pressure to 4-5 MPa, and naturally cool to room temperature to obtain a lysed suspension; place the lysed suspension in a high-speed refrigerated centrifuge , centrifuge at -20~-15°C for 5~8min at 6000~7000r / min, remove the lower precipitate to obtain the upper layer, adjust the pH of the upper layer to 4~5 with a sulfuric acid solution with a mass fraction of 40%, and let it stand Precipitate for 12-18 hours, collect the supernatant to obtain the lysate; adjust the pH of the lysate to 2-3 with hydrochloric acid with a mass fracti...

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Abstract

The invention discloses a preparation method of a humic acid suspended liquid fertilizer and belongs to the technical field of fertilizer preparation. The preparation method disclosed by the inventionhas the benefits that mixed suspended sludge liquid of sweet potato starch wastewater and secondary sedimentation activated sludge is used as a raw material and is changed from wastes into valuablesthrough pyrolysis; in addition, sodium humate in the humic acid fertilizer and a mixed carboxylic acid monomer in a liquefaction dispersant are subjected to graft copolymerization reaction, the non-polar end is combined with the hydrophobic surfaces of humic acid solid particles, and a polar carboxylic group is outward, so that the liquefaction dispersant is prevented from producing the hard precipitation in the liquid fertilizer; in the invention, glycine is added as a nitrogen element carrier, so that nitrogen requirements can be provided for crops; carboxyl groups in amino acids have chelating abilities and can also play a role in regulating the growth of the crops; side reaction can be generated between acrylic acids in the liquefaction dispersant in the liquid fertilizer and maleic anhydride to form acrylate, so that the liquid fertilizer is semi-oily and is more easily adhered onto the leaf surfaces of the crops, the transpiration is effectively inhibited, and the absorption efficiency of nutrient elements by the crops is improved, therefore, the application prospect is wide.

Description

technical field [0001] The invention discloses a preparation method of a humic acid suspension type liquid fertilizer, which belongs to the technical field of fertilizer preparation. Background technique [0002] Liquid fertilizer, also known as fluid fertilizer, commonly known as liquid fertilizer, is a liquid product of one or more nutrients required by crops, generally with the theme of N, P, K or one of the three major nutrients. Many micronutrients are also often included. [0003] Liquid fertilizers have been developed for 200 years. There are many varieties, which can be roughly divided into two categories: liquid nitrogen fertilizer and liquid compound fertilizer. Liquid nitrogen fertilizers include nitrogen in ammonium, nitrate and amide states, such as liquid ammonia, ammonia water, ammonia compounds of ammonium nitrate and ammonia, ammonia compounds of urea and ammonia, etc. Liquid compound fertilizers contain two or three nutrients of N, P, and K, such as ammo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C05G3/00
CPCC05C5/02C05G3/00C05G5/27C05C9/00C05C11/00C05D9/00C05D9/02C05F5/002C05F5/004C05F7/00C05F11/00C05F17/00
Inventor 吴刚何伟仁陈可
Owner 吴刚
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