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Cryogenic rubber thermal insulation material and preparation method thereof

A thermal insulation, rubber technology, applied in sustainable manufacturing/processing, climate sustainability, chemical industry, etc., to achieve the effect of improving flexibility

Inactive Publication Date: 2018-08-24
WINCELL INSULATION CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The technical problem to be solved in the present invention is to design a cryogenic rubber thermal insulation material and its preparation method to solve the existing technical problems

Method used

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  • Cryogenic rubber thermal insulation material and preparation method thereof
  • Cryogenic rubber thermal insulation material and preparation method thereof
  • Cryogenic rubber thermal insulation material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] (1) According to EPDM 15kg, butyl rubber (IIR) 5kg, butadiene rubber (BR) 5kg, high temperature foaming agent (AC) 10kg, antimony trioxide (Sb2o3) 5kg, zinc oxide 0.5kg, dioctyl ester (DOP) 10kg, antioxidant (4020) 0.1kg, antioxidant (AST-500) 1.2kg, microsphere foaming agent (F-82) 1.5kg, protective wax (HGB-3) 1kg, polyethylene glycol (PEG) 1kg, stearic acid 0.1kg, aluminum hydroxide 15kg, antioxidant (RD) 0.3kg, anti-scorch agent (PVI) 0.2kg, sulfur 0.2kg, diethylenedithiocarbamic acid The weight of zinc (E) 0.2kg and zinc dibutyl dithiocarbamate (B) 0.3kg takes raw materials;

[0025] (2) High temperature rubber mixing: the weighed EPDM rubber (EPDM), butyl rubber (IIR), butadiene rubber (BR), high temperature foaming agent (AC), antimony trioxide (Sb2o3) , zinc oxide, dioctyl (DOP), antiaging agent (4020), antioxidant (AST-500), protective wax (HGB-3), polyethylene glycol (PEG), stearic acid, aluminum hydroxide, Anti-aging agent (RD) and anti-scorch agent (PVI) a...

Embodiment 2

[0033] (1) According to EPDM 18kg, butyl rubber (IIR) 6kg, butadiene rubber (BR) 6kg, high temperature foaming agent (AC) 11kg, antimony trioxide (Sb2o3) 5kg, zinc oxide 0.6kg, dioctyl ester (DOP) 11kg, antioxidant (4020) 0.1kg, antioxidant (AST-500) 1.4kg, microsphere foaming agent (F-82) 1.7kg, protective wax (HGB-3) 1.2kg, polyethylene glycol (PEG) 1.2kg, stearic acid 0.2kg, aluminum hydroxide 16kg, antioxidant (RD) 0.4kg, anti-scorch agent (PVI) 0.3kg, sulfur 0.3kg, diethylene disulfide The weight of zinc substituted carbamate (E) 0.2kg and dibutyl dithiocarbamate zinc (B) 0.4kg takes raw materials;

[0034] (2) High temperature rubber mixing: the weighed EPDM rubber (EPDM), butyl rubber (IIR), butadiene rubber (BR), high temperature foaming agent (AC), antimony trioxide (Sb2o3) , zinc oxide, dioctyl (DOP), antiaging agent (4020), antioxidant (AST-500), protective wax (HGB-3), polyethylene glycol (PEG), stearic acid, aluminum hydroxide, Anti-aging agent (RD) and anti-sco...

Embodiment 3

[0042] (1) According to EPDM 21kg, butyl rubber (IIR) 7kg, butadiene rubber (BR) 7kg, high temperature foaming agent (AC) 12kg, antimony trioxide (Sb2o3) 6kg, zinc oxide 0.7kg, dioctyl ester (DOP) 12kg, antioxidant (4020) 0.3kg, antioxidant (AST-500) 1.6kg, microsphere foaming agent (F-82) 1.9kg, protective wax (HGB-3) 1.8kg, polyethylene glycol (PEG) 1.5kg, stearic acid 0.2kg, aluminum hydroxide 17kg, antioxidant (RD) 0.4kg, anti-scorch agent (PVI) 0.3kg, sulfur 0.3kg, diethylene dithio The weight of zinc carbamate (E) 0.3kg and zinc dibutyldithiocarbamate (B) 0.3kg takes raw materials;

[0043] (2) High temperature rubber mixing: the weighed EPDM rubber (EPDM), butyl rubber (IIR), butadiene rubber (BR), high temperature foaming agent (AC), antimony trioxide (Sb2o3) , zinc oxide, dioctyl (DOP), antiaging agent (4020), antioxidant (AST-500), protective wax (HGB-3), polyethylene glycol (PEG), stearic acid, aluminum hydroxide, Anti-aging agent (RD) and anti-scorch agent (PVI) ...

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Abstract

The invention relates to a cryogenic rubber thermal insulation material and a preparation method thereof. The thermal insulation material is prepared from the following components in parts by weight:15-25 parts of EPDM (ethylene propylene diene monomer), 5-10 parts of IIR (isobutylene isoprene rubber), 5-10 parts of BR (butadiene rubber), 10-15 parts of a high-temperature foamer (AC), 5-8 parts of Sb2O3, 0.5-1 part of zinc oxide, 0.2-0.4 parts of sulfur, 10-15 parts of DOP (diocty phthalate), 0.2-0.4 parts of zinc diethyldithiocarbamate (E), 0.1-0.4 parts of an anti-aging agent (4020), 1.2-2parts of an antioxidant (AST-500). Flexibility and elasticity are improved by substituting a traditional rubber-plastic foam product for a full rubber foam product; meanwhile, with adoption of the preparation method, the product can be resistant to ultraviolet rays, and aging resistance is enhanced. Besides, an added microballoon foamer is adopted for changing the foam structure to lock the air, and the material is more energy-saving and thermal-insulating. The material can keep soft, bent and elastic at low temperature, and is the thermal-insulating, non-corrosive and environment-friendly product.

Description

technical field [0001] The invention relates to the application field of thermal insulation materials, in particular to a cryogenic rubber thermal insulation material and a preparation method thereof. Background technique [0002] The thermal insulation materials on the market today generally use closed-cell materials, such as polyurethane, foam glass, polyisocyanurate, rubber and plastic insulation materials, etc. In the field of ultra-low temperature, due to the problems of condensed water and low temperature, these traditional thermal insulation materials are Hard materials will cause many problems during use, such as the treatment of the joints of hard materials, the process of thermal expansion and contraction of pipelines, or impacts that may cause material fragmentation and failure, material cutting, and inconvenient construction. . Cryogenic rubber thermal insulation material, its main feature is flexible material, easy to construct, and can still maintain a certain...

Claims

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Application Information

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IPC IPC(8): C08L23/16C08L23/22C08L9/00C08L91/06C08K13/02C08K3/22C08K3/06C08K5/39C08K5/09C08J9/10C08J9/32
CPCC08J9/103C08J9/32C08J2203/04C08J2203/18C08J2203/22C08J2323/16C08J2409/00C08J2423/22C08J2491/06C08K2201/014Y02P20/10
Inventor 秦伯军张君秦天德刘远斌曹鑫
Owner WINCELL INSULATION CO LTD
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