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FeCoVWNbSc high-entropy alloy powder used for laser cladding and use method

A high-entropy alloy and laser cladding technology, applied in metal material coating process, coating and other directions, can solve the problems of larger sample size, low bonding strength, lower cost, etc., to reduce high temperature brittleness, no cracks, The effect of good macroscopic topography

Active Publication Date: 2018-08-03
KUNMING UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] At present, research on high-entropy alloys mainly uses vacuum melting and casting to prepare bulk materials. cost increase in the sampling process, while laser cladding noble and gold can not only ensure excellent performance, but also effectively reduce costs
Although some scholars have prepared noble and gold coatings by means of magnetron sputtering and chemical deposition, but because the bonding method is usually physical bonding or mechanical bonding, the bonding strength between the coating and the substrate is low, and laser Cladding can not only form a metallurgical bond between the substrate and the coating to increase the bonding strength, but also effectively control the thickness of the coating, up to a few millimeters

Method used

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  • FeCoVWNbSc high-entropy alloy powder used for laser cladding and use method
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  • FeCoVWNbSc high-entropy alloy powder used for laser cladding and use method

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Effect test

Embodiment 1

[0022] The high-entropy alloy material in this embodiment is composed of six elemental powders of Fe, Co, V, W, Nb, and Sc, and the molar ratio of each component is: 1:1:1:1:1:0.02, and analyzed Electronic weighing of various metal element powders, the total mass of the metal powder is 50g, and the masses of the metal powder are: Fe: 6.30773g, Co: 6.64564g, V: 5.74453g, W: 10.47532g, Nb: 20.72537g, Sc: 0.10181g.

[0023] The preparation method of the high-entropy alloy material cladding layer of this embodiment includes the following steps:

[0024] (1) After mixing the various powders, perform vacuum ball milling for 3.5 hours and fully mix to obtain alloy powder with a particle size of 200-300 mesh.

[0025] (2) The base material is made of 45 steel, which is mechanically polished to remove oxides, acetone is used to remove oil stains, and ultrasonic alcohol is used for cleaning.

[0026] (3) The alloy powder material obtained in step (1) is uniformly pressed on the surface of the ...

Embodiment 2

[0030] The high-entropy alloy material in this embodiment is composed of six elemental powders of Fe, Co, V, W, Nb, and Sc, and the molar ratio of each component is: 1:1:1:1:1:0.025, and analyzed Electronic weighing of various metal element powders, the total mass of the metal powder is 50g, the masses of the metal powder are: Fe: 6.30453g, Co: 6.64227g, V: 5.74163g, W: 10.47003g, Nb: 20.71489g, Sc: 0.12665g.

[0031] The preparation method of the high-entropy alloy material cladding layer of this embodiment includes the following steps:

[0032] (1) After mixing each powder, perform vacuum ball milling, ball milling for 3 hours, and mixing thoroughly to obtain alloy powder with a particle size of 204-310 mesh.

[0033] (2) The base material is made of 45 steel, which is mechanically polished to remove oxides, acetone is used to remove oil stains, and ultrasonic alcohol is used for cleaning.

[0034] (3) The alloy powder material obtained in step (1) is uniformly pressed on the surfa...

Embodiment 3

[0038] The high-entropy alloy material in this embodiment is composed of six elemental powders of Fe, Co, V, W, Nb, and Sc. The molar ratio of each component is 1:1:1:1:1:0.03, and the analysis is adopted Weigh various metal element powders by electronic weighing, the total mass of metal powder is 50g, the masses of metal powder are: Fe: 6.30134g, Co: 6.63991g, V: 5.38772g, W: 10.46472g, Nb: 20.7044g, Sc: 0.15191g.

[0039] The preparation method of the high-entropy alloy material cladding layer of this embodiment includes the following steps:

[0040] (1) After mixing the various powders, perform vacuum ball milling for 3.5 hours and fully mix to obtain alloy powder with a particle size of 200-300 mesh.

[0041] (2) The base material is made of 45 steel, which is mechanically polished to remove oxides, acetone is used to remove oil stains, and ultrasonic alcohol is used for cleaning.

[0042] (3) The alloy powder material obtained in step (1) is uniformly pressed on the surface of t...

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Abstract

The invention discloses FeCoVWNbSc high-entropy alloy powder used for laser cladding and a use method, and belongs to the technical field of laser surface modification. The FeCoVWNbSc high-entropy alloy powder comprises the following components of Fe, Co, V, W, Nb and Sc, wherein the molar ratio of Fe to Co to V to W to Nb to Sc is 1:1:1:1:1:0.02:0.04; Sc is added in a quinary alloy of Fe, Co, V,W and Nb, so that the elements react with one another to present excellent high-temperature-oxidation-resistance, corrosion-resistance and the like, and the structure of a coating is excellent; a finedilution can also be formed by the coating and a substrate through laser cladding, so that metallurgical combination is formed; a good combination effect is formed between the substrate and the coating, and durability of the coating is favorably improved.

Description

Technical field [0001] The invention relates to a FeCoVWNbSc high-entropy alloy powder for laser cladding and a use method thereof, belonging to the technical field of laser surface modification. technical background [0002] Traditional alloys use one element as the main element (called principal element), and the properties of the alloy are improved by adding appropriate amounts of other elements. High-entropy alloys, also known as multi-principal alloys, are composed of 5-13 elements. The molar ratio of each element is between 5% and 35%. The properties of the alloy are determined by the combined action of multiple principal elements. High-entropy alloys with high strength, high hardness, high temperature softening resistance and high corrosion resistance can be obtained through proper composition design, which has important application prospects in certain special working environments (such as aviation, aerospace, energy and other fields). [0003] At present, the research on ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C24/10C22C30/00
CPCC22C30/00C23C24/106
Inventor 刘洪喜石海张晓伟刘子峰
Owner KUNMING UNIV OF SCI & TECH
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