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Preparation method of laminated glass glue with high bonding strength

A laminated glass, strength technology, applied in the direction of polymer adhesive additives, non-polymer adhesive additives, adhesives, etc., can solve the problems of low bonding strength, difficult fast curing, etc., and achieve the effect of improving bonding strength

Inactive Publication Date: 2018-06-15
陈合华
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The technical problem to be solved by the present invention is to provide a method for preparing laminated glass glue with high adhesion strength in view of the defects of low bonding strength and difficulty in fast curing of ordinary laminated glass glue

Method used

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  • Preparation method of laminated glass glue with high bonding strength

Examples

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Effect test

example 1

[0023] Mix silane coupling agent KH-560, anhydrous isopropanol and deionized water in a volume ratio of 3:1:2 and put them in a beaker for hydrolysis reaction for 16 minutes to obtain a self-made hydrolyzate. Silica sol with a mass fraction of 15% and The self-made hydrolyzate was mixed in a container at a volume ratio of 1:2, and mixed and reacted at a temperature of 65°C for 1 hour to obtain a modified silica sol; weigh 45 mL of polycaprolactone diol with a mass fraction of 15% and add it to the container In a four-necked flask with a stirrer, a thermometer and a condenser tube, stir at a temperature of 80° C. for 16 minutes, then dehydrate under reduced pressure for 45 minutes to obtain a stirred product, and then add toluene diisocyanate with a stirred product mass of 8% to the four-necked flask, Continue to insulate and mix the reaction for 16 minutes to obtain the reaction solution, and continue to mix the reaction solution, hydroxyethyl acrylate, hydroquinone and 20% hyd...

example 2

[0025]The silane coupling agent KH-560, anhydrous isopropanol and deionized water were mixed in a beaker with a volume ratio of 3:1:2 and hydrolyzed for 18 minutes to obtain a self-made hydrolyzate. Silica sol with a mass fraction of 15% and The self-made hydrolyzate was mixed in a container at a volume ratio of 1:2, and mixed and reacted at a temperature of 70°C for 2 hours to obtain a modified silica sol; 55 mL of polycaprolactone diol with a mass fraction of 15% was weighed and added to the container In a four-necked flask with a stirrer, a thermometer and a condenser tube, stir at a temperature of 90°C for 18 minutes, then dehydrate under reduced pressure for 50 minutes to obtain a stirred substance, then add toluene diisocyanate with a stirring substance mass of 8% to the four-necked flask, Continue to insulate and mix the reaction for 18 minutes to obtain the reaction solution. Continue to mix the reaction solution, hydroxyethyl acrylate, hydroquinone and 20% hydrogen per...

example 3

[0027] Mix silane coupling agent KH-560, anhydrous isopropanol and deionized water in a volume ratio of 3:1:2 and put them in a beaker for hydrolysis reaction for 20 minutes to obtain a self-made hydrolyzate. Silica sol with a mass fraction of 15% and The self-made hydrolyzate was mixed in a container at a volume ratio of 1:2, and mixed and reacted at a temperature of 75°C for 3 hours to obtain a modified silica sol; 65 mL of polycaprolactone diol with a mass fraction of 15% was weighed and added to the container In a four-necked flask with a stirrer, a thermometer and a condenser tube, stir at a temperature of 100° C. for 20 minutes, and then dehydrate under reduced pressure for 60 minutes to obtain a stirred substance, and then add toluene diisocyanate with a stirring substance mass of 8% to the four-necked flask, Continue to insulate and mix the reaction for 20 minutes to obtain the reaction solution, and continue to mix the reaction solution, hydroxyethyl acrylate, hydroqui...

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Abstract

The invention discloses a preparation method of laminated glass glue with high bonding strength, and belongs to the technical field of glass glue preparation. According to the preparation method provided by the invention, a self-made polyurethane acrylate prepolymer is used as a matrix, modified silica sol and self-made fruit wine are used as reinforcing substances, and the laminated glass glue isprepared with the supplement of a coupling agent and modified self-made reaction materials. Contained acrylates have double bounds with polymerization reaction activity, and free radicals can be polymerized under the action of illumination, so that crosslinking and solidification are carried out among polyurethane acrylate macromolecular chains, and the bonding strength is improved. According tothe preparation method, in the process of polymerization reaction, due to the steric hindrance effect of methyl in toluene diisocyanate molecules, the para-position reaction activity is usually largerthan the ortho-position reaction activity, and an effect of fast crosslinking and solidification is exerted. According to the preparation method, the silica sol is modified by a silane coupling agentand an alcohol solution, so that the bonding strength is strengthened by a network structure, the bonding property between the laminated glass glue and glass is enhanced, and thus the preparation method has a wide application prospect.

Description

technical field [0001] The invention discloses a preparation method of high bonding strength laminated glass glue, which belongs to the technical field of glass glue preparation. Background technique [0002] Laminated glass glue, also known as laminated safety glass glue, is a one-component anaerobic light-curing laminated glass glue, Doyer purple light modified acrylate adhesive, which is a colorless and transparent liquid, which is cured by isolating sunlight, ultraviolet rays and oxygen. . The material is endowed with a variety of unique functional properties, such as sound insulation, antistatic, vibration reduction, noise reduction, wave absorption, anti-aging, impact resistance and other properties. [0003] Laminated glass is a composite material in which glass and glass are separated by an intermediate layer and bonded together through treatment. It is generally used for the manufacture of safety glass, bulletproof glass, architectural decorative glass, art glass, ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J175/14C09J11/04C09J11/06C09J11/08C08G18/76C08G18/67C08G18/42C08G18/32C08G18/12
CPCC08G18/12C08G18/3215C08G18/4277C08G18/672C08G18/7614C08K2201/011C09J11/04C09J11/06C09J11/08C09J175/14C08L93/04C08K13/06C08K9/06C08K9/04C08K3/36C08K5/5425
Inventor 陈合华杨亚生陈可
Owner 陈合华
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