Method for preparing benzaldehyde catalyst through catalytic oxidation of benzyl alcohol
A catalytic oxidation and catalyst technology, which is applied in catalyst activation/preparation, organic compound preparation, physical/chemical process catalysts, etc., can solve the problems of complex process and corrosive damage of reaction equipment, and achieves low cost of raw materials and a wide range of applications. Wide and controllable shell thickness
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Embodiment 1
[0014] A kind of preparation method of benzaldehyde catalyst by catalytic oxidation of benzyl alcohol, the method comprises the following steps:
[0015] Step 1, 2molLa 2 o 3 @COF, 20mol propylene oxide, 1mol hydrochloric acid, 100mol deionized water, 20mol anhydrous
[0016] Ethanol was mixed evenly and stirred at 45°C for 60 minutes to obtain a clear transparent solution;
[0017] Step 2, add ammonia water to the above transparent solution to adjust the pH value of the mixed solution to 8.5, and continue to stir evenly at 50°C to obtain a colorless transparent solution; the obtained La 2 o 3 The @COF sol solution was poured into the mold and placed in a 50°C oven for 3 hours to obtain milky white La 2 o 3 @COF wet gel;
[0018] Step 3, add ethanol aging solution to the sample in the mold for aging treatment, replace the solvent 3 times, each time for 24 hours, and finally obtain milky white La 2 o 3 @COF alcohol gel;
[0019] Step 4, and then La 2 o 3 @COF alcohol...
Embodiment 2
[0024] Step 1, 1molLa 2 o 3 @COF, 2mol propylene oxide, 1mol hydrochloric acid, 100mol deionized water, 20mol anhydrous
[0025] Ethanol was mixed evenly at 45°C and stirred for 60 minutes to obtain a clear transparent solution; the rest of the steps were the same as in Example 1.
Embodiment 3
[0027] Step 1, the 4molLa 2 o 3 @COF, 1mol propylene oxide, 1mol hydrochloric acid, 100mol deionized water, 20mol anhydrous
[0028] Ethanol was mixed evenly at 45°C and stirred for 60 minutes to obtain a clear transparent solution; the rest of the steps were the same as in Example 1.
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