Clothing nursing agent, and preparation method thereof
A technology of clothing care and additives, which is applied in fiber treatment, wear-resistant fibers, and improved hand-feeling fibers, etc. It can solve problems such as pilling, fading, and hardening of clothing fabrics, and achieve color retention, reduce directional friction effects, The effect of improving color fixing performance
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example 1
[0025] Clothing care agent auxiliary A is to add chloroplatinic acid to isopropanol at a mass ratio of 1:25, and stir at 40°C for 0.5h to obtain a catalyst. 12 parts of ether, 5 parts of catalyst, 9 parts of hydrogen-terminated silicone oil, nitrogen gas, react at 80°C for 5 hours to obtain reactant A, take reactant A at a mass ratio of 5:1, add 3-dimethylaminopropylamine and heat to 45°C Keep warm for 3 hours to obtain clothing care agent auxiliary agent A.
[0026] Clothing care agent auxiliary agent B is calculated in parts by mass. Take 10 parts of n-octylamine, 15 parts of dodecyl primary amine, and 11 parts of hydrochloric acid with a mass fraction of 36% are stirred and mixed to obtain a mixed solution, and the mixed solution is added to The cyanamide solution with a fraction of 50% and dicyandiamide were stirred and refluxed, distilled under reduced pressure, and vacuum-dried to obtain a dried product. Acetone was added to the dried product for recrystallization to obt...
example 2
[0032]Clothing care agent auxiliary A is to add chloroplatinic acid to isopropanol at a mass ratio of 1:25, stir at 55°C for 1 hour to obtain a catalyst, and take allyl alcohol polyoxyethylene epoxy group-terminated polyether in parts by mass 14 parts, 7 parts of catalyst, 10 parts of hydrogen-terminated silicone oil, pass nitrogen gas, react at 100°C for 6 hours to obtain reactant A, take reactant A and add 3-dimethylaminopropylamine at a mass ratio of 5:1, heat to 55°C and keep it warm 4h, the clothing care agent additive A was obtained.
[0033] Clothing care agent auxiliary agent B is calculated in parts by mass. Get 12 parts of n-octylamine, 18 parts of dodecyl primary amine, and 13 parts of hydrochloric acid with a mass fraction of 36% are stirred and mixed to obtain a mixed solution. Take the mixed solution and add mass fraction The cyanamide solution with a fraction of 50% and dicyandiamide were stirred and refluxed, distilled under reduced pressure, and vacuum-dried t...
example 3
[0039] Clothing care agent auxiliary A is to add chloroplatinic acid to isopropanol at a mass ratio of 1:25, and stir at 47°C for 0.75h to obtain a catalyst. 13 parts of ether, 6 parts of catalyst, 9.5 parts of hydrogen-terminated silicone oil, nitrogen gas, and react at 90°C for 5.5 hours to obtain reactant A. Take reactant A and add 3-dimethylaminopropylamine at a mass ratio of 5:1 and heat to 50 ℃ for 3.5 hours to obtain clothing care agent auxiliary agent A.
[0040] Clothing care agent auxiliary agent B is calculated in parts by mass. Take 11 parts of n-octylamine, 16.5 parts of dodecyl primary amine, and 12 parts of hydrochloric acid with a mass fraction of 36% are stirred and mixed to obtain a mixed solution, and the mixed solution is added to The cyanamide solution with a fraction of 50% and dicyandiamide were stirred and refluxed, distilled under reduced pressure, and vacuum-dried to obtain a dried product. Acetone was added to the dried product for recrystallization ...
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