Preparation method of copper/graphite film multi-layer laminated blocky composite material
A composite material and graphite technology, applied in metal layered products, chemical instruments and methods, layered products, etc., can solve the problems of low interlayer strength of graphite films, non-bonding of copper and graphite film interfaces, etc., and achieve a wide range of applications. Effect
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Embodiment 1
[0020] Configure a mixture of polyvinyl butyral and ethanol as a binder, pour copper powder and stir evenly to form a slurry, and drop in dimethyl phthalate as a plasticizer; stir the slurry evenly and pour it into the casting machine, adjust the height of the blade to 40 μm, spread evenly on the mesh graphite film, the mesh size of the graphite film is 1mm, and the interval is 2mm; the cast film that has been formed is placed in a vacuum drying oven to dry, and then degummed, cut, Stacked, put into a graphite mold for pressure sintering, the sintering temperature is 1000°C, the pressure is 5MPa, and a dense block composite material is prepared; the volume fraction of graphite film in the composite material is 50vol%, and the density of the composite material is measured by the drainage method 5.52g / cm 3 , the thermal conductivity of the composite material measured by the laser flash method is 590W / mK.
Embodiment 2
[0022] Configure a mixture of polyvinyl butyral and ethanol as a binder, pour copper powder and stir evenly to form a slurry, and drop in dimethyl phthalate as a plasticizer; stir the slurry evenly and pour it into the casting machine, adjust the height of the blade to 80 μm, spread evenly on the mesh graphite film, the mesh size of the graphite film is 1mm, and the interval is 2mm; the cast film that has been formed is placed in a vacuum drying oven to dry, and then degummed, cut, Stacked, put into a graphite mold for pressure sintering, the sintering temperature is 1000°C, the pressure is 5MPa; the volume fraction of graphite film in the composite material is 35vol%, and the density of the composite material measured by the drainage method is 6.53g / cm 3 , the thermal conductivity of the composite material was measured to be 497W / mK by laser flash method.
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