Horseradishtree leaf water-soluble extractive with good mouth feel, characteristic horseradishtree leaf taste and taste similar to tea, and extraction method of extractive
A technology of water-soluble extract and Moringa leaf, which is applied in the field of extraction technology and food, and can solve problems such as poor taste
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Embodiment 1
[0018] Extraction process: weighing plant material→reflux extraction→filtering→combining filtrates→concentrating under reduced pressure→freeze-drying→calculating yield→sensory evaluation→water solubility evaluation→choose the optimal process for 3 repeated experiments.
[0019] Sensory evaluation method: The extract is accurately weighed and formulated into a certain concentration to be tested. The sensory evaluation team composed of professional screening evaluates the taste activity of the samples, and each sample is repeated 3 times.
[0020] Extraction of ethanol and water extract: get dried Moringa oleifera leaves, pulverize, cross 20 mesh sieves, accurately weigh 50g, totally 5 parts, use 95%, 80%, 50%, 30% ethanol-water cold soaking extraction and Distilled water heating and reflux extraction (both 500ml, sequentially numbered A-E), extraction times 3 times, filtered, combined filtrates, concentrated under reduced pressure to a small volume, dried with a freeze dryer, to...
Embodiment 2
[0036] Analysis of the volatile components of the extract:
[0037] Analytical instrument: Agilent 7890A-5975C gas chromatography-mass spectrometry (GC-MS).
[0038] Solid phase microextraction equipment: supelco solid phase microextraction handle and adsorption column.
[0039] GC-MS analysis method: gas phase conditions: chromatographic column: Agilent 19091J-115, HP-5 (5% PhenylMethyl Siloxan, 50m×0.32mm×0.52μm); inlet temperature: 250°C; oven temperature program: 40°C Keep for 5 minutes, then rise to 250°C by 5 degrees per minute, and keep for 10 minutes; injection volume: 1 microliter; split ratio: splitless; inlet pressure: 87 kPa; flow rate: 1.8 ml / min.
[0040] Mass spectrometry conditions: ionization mode EI, electron bombardment energy 70eV, scanning range 20-500nm; quantitative method: relative peak area normalization method; spectral library: NIST 08.
[0041] Sample collection: Accurately weigh 2g of the extract ⑤ in Example 1, put it in a 10ml headspace bottle,...
Embodiment 3
[0047] Moringa leaf extract drink:
[0048] Formula: Moringa leaf extract 0.25%, white sugar 2%, honey 0.8%, citric acid 0.005%, edible purified water. The moringa leaf extract, white granulated sugar, honey and citric acid are accurately weighed in proportion and dissolved in purified drinking water, filled and sterilized to obtain the natural moringa leaf extract beverage.
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