Acephate pesticide
A technology of acephate and methamidophos, which is applied in the directions of pesticides, animal repellents, botanical equipment and methods, etc., can solve the problems of human and animal poisoning, improper storage and use, etc., and achieves low cost and resistance to resistance. Good medicinal properties and stability
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Embodiment 1
[0014] A kind of acephate pesticide, each component by weight: 100 parts of acephate, 5 parts of hexaflumuron, 20 parts of cyhalothrin, 0.5 parts of stabilizer, 5 parts of emulsifier and 20 parts of toluene solvent share. The emulsifier is one or more of nonylphenol polyoxyethylene ether, alkylbenzene calcium sulfate, and styrene-ethylphenyl polyoxyethylene-polyoxypropylene ether.
[0015] The preparation process of acephate comprises the steps:
[0016] (1) Put methamidophos and chloroform into the reaction kettle according to the molar ratio of 1:1, stir evenly, then add acetyl chloride dropwise, the molar ratio of methamidophos and acetyl chloride is 1:1.5, and control the vacuum -0.04MPa, the hydrogen chloride gas released by the reaction is absorbed by water to produce hydrochloric acid; (2) After the reaction is completed, the obtained reaction solution is subjected to precipitation, the precipitation temperature is 70-75°C, the vacuum is -0.15MPa, and the precipitation...
Embodiment 2
[0018] A kind of acephate pesticide, each component by weight: 125 parts of acephate, 10 parts of hexaflumuron, 25 parts of cyhalothrin, 1.0 parts of stabilizer, 6 parts of emulsifier and 35 parts of toluene solvent share. The emulsifier is one or more of nonylphenol polyoxyethylene ether, alkylbenzene calcium sulfate, and styrene-ethylphenyl polyoxyethylene-polyoxypropylene ether.
[0019] The preparation process of acephate comprises the steps:
[0020] (1) Put methamidophos and chloroform into the reaction kettle according to the molar ratio of 1:1, stir evenly, then add acetyl chloride dropwise, the molar ratio of methamidophos and acetyl chloride is 1:1.5, and control the vacuum -0.04MPa, the hydrogen chloride gas released by the reaction is absorbed by water to produce hydrochloric acid; (2) After the reaction is completed, the obtained reaction solution is subjected to precipitation, the precipitation temperature is 70-75°C, the vacuum is -0.15MPa, and the precipitatio...
Embodiment 3
[0022] A kind of acephate pesticide, each component by weight: 140 parts of acephate, 12 parts of hexaflumuron, 27 parts of cyhalothrin, 1.2 parts of stabilizer, 7 parts of emulsifier and 40 parts of toluene solvent share. The emulsifier is one or more of nonylphenol polyoxyethylene ether, alkylbenzene calcium sulfate, and styrene-ethylphenyl polyoxyethylene-polyoxypropylene ether.
[0023] The preparation process of acephate comprises the steps:
[0024] (1) Put methamidophos and chloroform into the reaction kettle according to the molar ratio of 1:1, stir evenly, then add acetyl chloride dropwise, the molar ratio of methamidophos and acetyl chloride is 1:1.5, and control the vacuum -0.04MPa, the hydrogen chloride gas released by the reaction is absorbed by water to produce hydrochloric acid; (2) After the reaction is completed, the obtained reaction solution is subjected to precipitation, the precipitation temperature is 70-75°C, the vacuum is -0.15MPa, and the precipitatio...
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